在FeCo磁性合金中异常粒的表征
Julia I Deitz1, Timothy J Ruggles1, Philip J Noell1
1Materials Characterization and Performance Department, Sandia National Laboratories, 1515 Eubank Blvd. SE - Mail Stop 1411 - Albuquerque, NM 87123, USA.
概括
电子道对比成像 (ECCI) 揭示了热处理的FeCo合金中带有脱位网络的未再结晶的颗粒. 这些缺陷作为塑料变形的障碍,为合金故障机制提供了洞察力.
科学领域:
- 材料科学 材料科学 材料科学
- 金工业是金工业的一个方面.
- 电子显微镜电子显微镜
背景情况:
- 热处理的FeCo基磁合金需要详细的结构特征.
- 了解微结构缺陷对于预测合金性能至关重要.
研究的目的:
- 用电子显微镜来描述热处理的FeCo合金的结构性质.
- 调查独特的粒度结构和合金行为缺陷的作用.
主要方法:
- 扫描电子显微镜 (SEM) 使用电子道对比成像 (ECCI).
- 高分辨率的电子反散衍射 (HR-EBSD).
- 微内测试. 微内测试. 微内测试. 微内测试.
主要成果:
- ECCI确定了具有网状脱位网络和亚粒边界的独特的谷物.
- 这些特征被确定为未再结晶的粒.
- 脱位网络阻碍了滑带的传播,作为阻碍塑料变形的障碍.
结论:
- ECCI是一种快速的方法,用于量化合金中的未再结晶的颗粒.
- 脱位网络显著影响FeCo合金中的塑性变形和脆性失效机制.
- ECCI提供了有关合金故障机制的宝贵见解.
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