在线XRF分析仪用于测量酸盐泥中的P2O5含量
Ismail Ben Amar1,2,3, Andrew Thomas4, Claus Bachmann4
1Department of Electrical and Computer Engineering, Université Laval, Quebec City, QC, Canada. ismail.ben-amar.1@ulaval.ca.
Scientific reports
|October 20, 2023
概括
一个优化的在线X射线光 (XRF) 设置准确地分析酸盐泥 (PS) P2O5含量. 水平流配置实现了低平均绝对误差,证明了XRF.
科学领域:
- 分析化学 分析化学
- 材料科学 材料科学 材料科学
背景情况:
- 在酸盐泥中精确的P2O5分析对于工艺控制至关重要.
- 在线分析为化学工业的实时监控提供了优势.
研究的目的:
- 构建和优化在线X射线光 (XRF) 设置,用于酸盐泥 (PS) 中的P2O5分析.
- 评估不同的流量配置,以提高准确性和效率.
- 为在线P2O5测定确定最佳测量参数.
主要方法:
- 在线XRF设置的构建和优化.
- 使用垂直和水平流配置对酸盐泥样品的分析.
- 使用参考样本开发校准曲线.
- 测量参数的实验优化 (刺激能量,电流,距离,时间,波器).
主要成果:
- 水平流配置实现了0.38%的平均绝对误差,明显优于垂直流 (0.87%).
- 对于高达18.50%的P2O5度 (水平流) 建立了校准曲线.
- 最佳参数包括20-25kV激发能量,600μA电流,18毫米的样品探测器距离,60秒的测量时间和过器.
结论:
- 优化的在线XRF设置是确定酸盐泥中P2O5含量的可行和准确方法.
- 横流配置为此应用提供了卓越的性能.
- 对于酸盐生产中化学分析的数字化,XRF技术显得有前途.
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