在单晶超合金的γ/γ'-微结构中的局部误导在爬行过程中的演变被用旋转向量基线 (RVB) EBSD方法研究
Stepan Gamanov1,2, A Dlouhy1, D Bürger3
1Institute of Physics of Materials, Czech Academy of Sciences, Brno, Czech Republic.
Microscopy research and technique
|November 8, 2023
概括
本研究使用RVB-EBSD来分析Ni基超合金在爬行过程中的误导. 它揭示了异位如何在相位边界形成和填充通道,为材料变形提供了洞察力.
科学领域:
- 材料科学 材料科学 材料科学
- 金工业是金工业的一个方面.
- 晶体学 晶体学是指结晶学.
背景情况:
- 基单晶超合金 (SXs) 对于高温应用至关重要.
- 变形显著改变了SXs.的微观结构.
- 了解相位边界误导是预测合金性能的关键.
研究的目的:
- 研究Ni-基SXs在爬行过程中玛和玛相之间的小误导的演化.
- 应用旋转向量基线电子反向散射方向成像 (RVB-EBSD) 方法用于高分辨率的微观结构分析.
- 记录在相位接口上的失位网络形成和行为.
主要方法:
- 使用RVB-EBSD进行精确的定向成像,准确度为0.01°.
- 结合晶体学和化学信息用于相分离.
- 在SX ERBO1 (CMSX4型) 中分析了微结构演变,在850°C和600MPa时的爬行后.
主要成果:
- 成功记录了在玛/玛'接口上脱位网络的形成.
- 观察到位填充马通道,与TEM发现一致.
- 量化了微观结构长度尺度上误导的演变.
结论:
- 定向成像对于研究SXs的爬行诱导的微观结构变化是有效的.
- RVB-EBSD提供了有关相位边界的脱位行为的宝贵数据.
- 这些发现提高了对Ni基超合金中的爬行机制的理解.
更多相关视频
07:37Full-field Strain Measurements for Microstructurally Small Fatigue Crack Propagation Using Digital Image Correlation Method
Published on: January 16, 2019
9.7K
11:14Comprehensive Characterization of Extended Defects in Semiconductor Materials by a Scanning Electron Microscope
Published on: May 28, 2016
13.9K
相关概念视频
Normal Strain under Axial Loading
537
Normal strain under axial loading is an important concept in the field of mechanics of materials. Axial loading implies the application of a force along the axis of a material, like a column or bar. This force can either compress or stretch the material. In the context of axial loading, normal strain is the deformation experienced by the material in the direction of the loading force. It's calculated as the change in length divided by the original length of the material. This unitless ratio...
537
Factors Affecting Creep
145
In normal-weight aggregate concrete, the hardened cement paste is the primary contributor to creep, whereas the aggregates, being stiffer than the cement paste, are more resilient to stress-induced deformation. The stiffness of the aggregates is defined by their modulus of elasticity, and the more voluminous they are in the concrete, the less it will creep.
Further, the water/cement ratio is critical, as a lower ratio increases concrete strength, thus reducing creep. The strength of the...
Further, the water/cement ratio is critical, as a lower ratio increases concrete strength, thus reducing creep. The strength of the...
145
Stress-Strain Diagram - Ductile Materials
789
The stress-strain relationship in ductile materials such as structural steel or aluminium is intricate and progresses through several stages. When a specimen is loaded, it initially exhibits a linear length increase, depicted by a steep straight line on the stress-strain diagram. It indicates the material is elastically deforming and will return to its original shape once unloaded. However, when a critical stress value is reached, plastic deformation begins. This stage sees substantial...
789
Elastic Strain Energy for Shearing Stresses
197
As discussed in previous lessons, strain energy in a material is the energy stored when it is elastically deformed, a concept crucial in materials science and mechanical engineering. This energy results from the internal work done against the cohesive forces within the material. When a material undergoes shearing stress and corresponding shearing strain, the strain energy density, which is the energy stored per unit volume, is calculated. Within the elastic limit, where the stress is...
197
Residual Stresses in Bending
178
In the study of elastoplastic members subjected to bending moments, understanding the loading and unloading phases is crucial for assessing material behavior and structural integrity. During the loading phase, as the bending moment increases, the material initially responds elastically, adhering to Hooke's Law, where stress is directly proportional to strain. When the load exceeds the yield strength, plastic deformation occurs, resulting in permanent strain and deformation that remains even...
178
Stress-Strain Diagram - Brittle Materials
2.5K
Brittle materials, including glass, cast iron, and stone, exhibit unique characteristics. They fracture without considerable change in their elongation rate, indicating that their breaking and ultimate strength are equivalent. Such materials also show lower strain levels at the point of rupture. The failure in brittle materials predominantly results from normal stresses, as evidenced by the rupture created along a surface perpendicular to the applied load. These materials do not display...
2.5K
