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一种基于ZnO装饰的聚氨酸/煤纳米复合材料的新型电位计传感器,用于化的确定

G A El Sayed¹, Mostafa R Abukhadra², S M Mostafa¹

¹Chemistry Department, Faculty of Science, Beni-Suef University Beni-Suef Egypt magdy_mmagdy@yahoo.com mohamed.mahmoud@science.bsu.edu.eg.

|November 30, 2023

概括

一种用 ZnO@PANI/C 纳米复合材料修改的新型碳糊传感器提供了一种敏感且稳定的方法来测定稀化. 这种电化学传感器在各种样本中实现了diltiazem的低检测极限.

科学领域:

电分析化学电分析化学
材料科学材料科学材料科学
纳米技术纳米技术

背景情况:

迪尔蒂亚泽姆 (DTZ) 是治疗心血管疾病的关键药物,如心痛,高血压和心律失常.
准确量化DTZ对于治疗药物监测和质量控制至关重要.

研究的目的:

开发一种高度灵敏和稳定的改性碳糊传感器,用于化的电位测量测定.
为了提高电化学性能并降低DTZ分析的检测极限.

主要方法:

一个碳糊传感器的制造,该传感器包含β-cyclodextrin,NaTPB和ZnO装饰的聚氨酸/煤纳米复合材料 (ZnO@PANI/C).
使用XRD,FT-IR和SEM进行纳米材料的表征;通过EIS分析的表面特性.
对DTZ进行电位测量测定,评估对干扰物质的敏感性,稳定性,可重复性和选择性.

主要成果:

开发的基于ZnO@PANI/C的传感器在Nernstian斜率下表现出色.
在1.0×10−6到1.0×10−2的线性范围内达到5.0×10−7molL−1的低检测极限.
传感器表现出快速响应时间 (≤10.0秒) 和高选择性,成功应用于制药和工业用水样本.

结论:

经过修改的碳糊传感器提供了可靠和高效的分析工具,用于化量化.
使用 ZnO@PANI/C 纳米复合材料显著提高了传感器性能,使其能够进行敏感的检测.
该方法在现实世界样本中的适用性突出了其在制药和环境分析中的实际价值.

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