意想不到的后果:评估因微计算机X射线断层成像而导致的烯泡的热力学变化
Alexander K Landauer1, Zois Tsinas1,2, Orion L Kafka3
1Material Measurement Laboratory, National Institute of Standards and Technology, 100 Bureau Drive, Gaithersburg, 20899, MD, USA.
概括
在现场微计算X射线断层扫描 (microCT) 期间的辐射暴露显著改变了乙烯酸泡的热物理,化学和机械性能. 这些变化影响结构与属性关系,但为材料设计提供了修改途径.
科学领域:
- 材料科学 材料科学 材料科学
- 聚合物科学 聚合物科学
- 机械工程 机械工程
背景情况:
- 微计算X射线断层扫描 (microCT) 对于材料结构分析至关重要.
- 在机械测试的现场微CT显示了应变引起的变化.
- 在in situ微CT过程中辐射对弹性质的影响还未得到研究.
研究的目的:
- 量化辐射剂量对乙烯酸泡性能的影响.
- 研究热,化学和机械特性中的变化.
- 在in situ微型CT中评估结构-财产关系的影响.
主要方法:
- 乙烯基酸泡暴露于不同剂量的辐射 (每天8.1kGy/d的0-3天).
- 使用扫描电子显微镜,差分扫描热量计,动态机械分析,里埃变换红外光谱学,能量分散式X射线光谱学和索克斯莱特提取的表征.
- 机械测试 (粘性弹性) 从-30°C到60°C.
主要成果:
- 增加的辐射剂量导致材料变硬,并增加了能量消散.
- 观察到热物理和化学性质的显著变化.
- 形态和化学结构的变化与属性修改相关.
结论:
- 在in situ微型CT过程中暴露于辐射会大大改变泡的特性,可能会混测量结果.
- 这些修改为调整材料性能提供了机会.
- 量化属性变化可以为有限元模型提供信息,以优化冲击保护设计.
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San Francisco's Golden Gate Bridge is exposed to temperatures ranging from -15 °C to 40 °C. At its coldest, the main span of the bridge is 1275 m long. Assuming that the bridge is made entirely of steel, what is the change in its length between these temperatures?
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