通过光学形计测量在水泥材料的样品制备过程中表面研磨的量化
Patrick Holthuizen1, Oğuzhan Çopuroğlu1
1Faculty of Civil Engineering & Geosciences, Section of Materials & Environment, Delft University of Technology, Delft, The Netherlands.
Journal of microscopy
|December 18, 2023
概括
适当的样本准备对于准确的显微镜和微观结构分析至关重要. 这项研究量化评估了水泥材料的研磨步骤,为扫描电子显微镜中改善表面质量提供了可重复的指导.
科学领域:
- 材料科学 材料科学 材料科学
- 分析化学 分析化学
- 地质地质地质地质地质地
背景情况:
- 准确的微观结构分析在很大程度上依赖于适当的样本准备用于显微镜.
- 在扫描电子显微镜 (SEM) 用能量分散光谱 (EDS) 量化时,获得精细抛光的表面至关重要.
- 使用聚合物制备水泥材料,由于材料异质性,因此面临着独特的挑战.
研究的目的:
- 量化评估磨砂参数在样本准备过程中对表面质量的影响.
- 为在显微镜样品制备过程中研磨和预抛光步骤提供可重复的指导.
- 解决目前在样本准备中的表面质量评估的主观性质的问题.
主要方法:
- 使用数字显微镜与光学分析对研磨的定量评估.
- 在每个研磨阶段后,逐步分析表面形状.
- 使用光学和电子显微镜评估表面质量.
主要成果:
- 研磨显著影响表面粗度和质量,在每一步后都有可测量的变化.
- 真空环氧浸有助于减轻像水泥材料这样的异质样本的削减.
- 该研究展示了一种量化方法来评估表面质量,超越主观评估.
结论:
- 研磨和预抛光步骤至关重要,并且在微镜样本准备过程中经常被低估.
- 表面形状的定量评估为优化样本准备提供了可重复的指导.
- 这项工作提供了一种标准化的方法,以提高水泥材料微结构分析的可靠性.
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