用四种不同的溶剂在immortelle水溶中溶解化合物的多次液体液体提取
Andreja Komnenić1, Zorica Lazarević2, Zoran Jovović1
1Department of Field and Vegetable Crops, Biotechnical Faculty in Podgorica, University of Montenegro, Mihaila Lalića 15, 81000, Podgorica, Montenegro.
Chemistry & biodiversity
|December 20, 2023
概括
分析了化品副产品Immortelle水溶的化学成分. 叶绿素被证明是最有效的提取挥发性化合物,揭示关键成分,并证明,即使在多次提取后,精油化合物仍然存在于水溶中.
科学领域:
- 分析化学 分析化学
- 植物化学 植物化学
- 化品科学 化品科学
背景情况:
- 不朽 (Helichrysum italicum) 精油在化品中受到重视.
- 不朽的水溶是一种副产品,尽管有极性活性成分的潜力,但仍未得到充分利用.
研究的目的:
- 为了研究immortelle水溶的化学成分.
- 评估不同溶剂的效率,从水溶中提取挥发性化合物.
- 为了确定提取的最佳数量,以最大限度地提高挥发性化合物回收.
主要方法:
- 液液提取 (LLE) 使用四种不同的非极性溶剂 (,二甲,六,).
- 在工业生产的不朽水溶上进行了十次连续的提取.
- 气色谱 (GC) 分析使用四度甘作为量化的内部标准.
主要成果:
- 形式是最有效的溶剂,提取了2447.0 mg/L的挥发性化合物.
- 确定的主要化合物包括3-pentanone,2-methyl-1-butanol和γ-terpineol.
- 挥发性化合物的最佳回收 (~92%) 在五个LLE周期内实现.
结论:
- 不朽的水溶含有有价值的挥发性有机化合物.
- 形式是从水溶中提取这些化合物的首选溶剂.
- 很大一部分精油化合物可以从水溶中有效地回收.
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