洋的地理来源歧视性分析:用于ICP-OES和ICP-MS分析的化学测量方法
Kyu Sang Sim1, Hyoyoung Kim1, Suel Hye Hur1
1National Agricultural Products Quality Management Service, Gimcheon 39660, Republic of Korea.
Food research international (Ottawa, Ont.)
|December 21, 2023
概括
诱导合血 (ICP) 分析与化学测量结合,准确地确定了洋的地理来源. 这种元素分析方法在区分韩国洋和中国洋方面实现了100%的准确性.
科学领域:
- 农业科学 农业科学
- 分析化学 分析化学
- 食品安全 食品安全
背景情况:
- 地理来源对农产品的质量和安全有重大影响.
- 准确的原产地确定对于消费者信任和监管合规性至关重要.
研究的目的:
- 开发和验证一种使用元素分析识别洋的地理来源的方法.
- 根据它们的无机元素形状来区分韩国洋和中国洋.
主要方法:
- 诱导合血 (ICP) 分析用于量化洋样本中的无机元素.
- 应用了化学测量技术,包括主要成分分析 (PCA),部分最小正方形歧视分析 (PLS-DA) 和直角部分最小正方形歧视分析 (OPLS-DA).
- 规范差别分析 (CDA) 用于最终的原产地确定.
主要成果:
- 正交部分最小方形差异分析 (OPLS-DA) 成功区分了韩国和中国洋群.
- 确定了17个关键元素,在预测 (VIP) 值中具有可变重要性≥1.
- 接收器操作特征 (ROC) 曲线显示曲线下面的面积 (AUC) 为1,表示完美的区分.
- 准则差别分析 (CDA) 在确定原产国时实现了100%的准确性.
结论:
- 开发的ICP-ICP和化学测量方法为区分洋的地理来源提供了非常准确的方法.
- 这种元素分析技术是验证农产品原产地,确保质量和安全的宝贵工具.
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