颗粒大小对三酸盐定性行为的影响:使用ISO 6876隙测试和同热感应热量计的比较研究
Anarela Vassen Bernardi1,2, Marcelo Tramontin Souza3, Oscar Rubem Klegues Montedo2
1Graduate Program in Dentistry, School of Dentistry, Federal University of Rio Grande do Sul (UFRGS), Porto Alegre 90010-150, RS, Brazil.
Bioengineering (Basel, Switzerland)
|January 22, 2024
概括
较小的三酸颗粒大小可以加速水泥水化,将定时间缩短高达24%. 隙测试和热量计显示出对设置时间评估的良好相关性,偏差低于12%.
科学领域:
- 材料科学 材料科学 材料科学
- 化学工程是化学工程的重要组成部分.
- 建筑材料 建筑材料
背景情况:
- 三酸盐 (C3S) 是波特兰水泥的主要组成部分.
- 颗粒大小显著影响水泥水化动力学和设置行为.
- 标准化方法对于可靠评估水泥材料性能至关重要.
研究的目的:
- 为了研究三酸颗粒大小对水泥置行为的影响.
- 为了比较ISO 6876缩影测试和同热热度计的结果.
- 为了确定颗粒大小和水泥位特征之间的相关性.
主要方法:
- 用水与固体比率为0.66.6的水制成的水泥糊.
- 设置时间使用ISO 6876的缩测试进行评估.
- 在室温下通过同热传导热量计监测水化动力学.
主要成果:
- 减少颗粒大小加速了水泥糊的水化,将定时间缩短了高达24%.
- 从缩测试开始的最终设置时间与热量计曲点非常相匹配.
- 在不同的粒子大小中,方法偏差始终低于12%.
结论:
- 颗粒大小是控制三酸盐水化和设置的关键因素.
- 根据ISO 6876标准,缩和同热热度计是设置时间评估的补充技术.
- 方法之间的准确相关性支持可靠的水泥材料的表征.
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