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Updated: Jul 2, 2025

Atomic Scale Structural Studies of Macromolecular Assemblies by Solid-state Nuclear Magnetic Resonance Spectroscopy
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对于1H检测到有机固体在快速MAS中中继的DNP的最佳灵敏度

Saumya Badoni1, Pierrick Berruyer1, Lyndon Emsley1

  • 1Institut des Sciences et Ingénierie Chimiques, Ecole Polytechnique Fédérale de Lausanne (EPFL), CH-1015 Lausanne, Switzerland.

Journal of magnetic resonance (San Diego, Calif. : 1997)
|February 24, 2024
PubMed
概括

动态核极化 (DNP) 增强了固态H NMR的敏感性. 最佳的魔法角旋转 (MAS) 速率平衡了超极化损失与线条缩小,以在质子固体中获得最大的灵敏度.

关键词:
动态核极化是指一个动态的核极化.快速的魔法角度旋转旋转继电动的动态核极化.固态NMR是一种固态NMR.

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