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相关概念视频

¹³C NMR: Distortionless Enhancement by Polarization Transfer (DEPT)01:20

¹³C NMR: Distortionless Enhancement by Polarization Transfer (DEPT)

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When proton-coupled carbon-13 spectra are simplified by a broadband proton decoupling technique, structural information about the coupled protons is lost. Distortionless enhancement by polarization transfer (DEPT) is a technique that provides information on the number of hydrogens attached to each carbon in a molecule. While the DEPT experiment utilizes complex pulse sequences, the pulse delay and flip angle are specifically manipulated. The resulting signals have different phases depending on...
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Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation01:26

Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation

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Inductively coupled plasma (ICP) is the common plasma source used in atomic emission spectroscopy (AES), a technique that detects and analyzes various elements in a sample. This method is often called inductively coupled plasma atomic emission spectroscopy (ICP-AES).
There are three main types of inductively coupled plasma atomic emission spectroscopy  (ICP-AES) instruments: sequential, simultaneous multichannel, and Fourier transform instruments, with the latter being less commonly used....
218
Atomic Emission Spectroscopy: Lab01:29

Atomic Emission Spectroscopy: Lab

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AES is a powerful analytical technique, especially effective when used with plasma sources, producing abundant spectra in characteristic emission lines. The Inductively Coupled Plasma (ICP), in particular, yields superior quantitative analytical data due to its high stability, low noise, low background, and minimal interferences under optimal experimental conditions. However, newer air-operated microwave sources are emerging as promising alternatives that could be more cost-effective than...
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Atomic Emission Spectroscopy: Overview01:20

Atomic Emission Spectroscopy: Overview

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Atomic emission spectroscopy (AES) is an analytical technique used to determine the elemental composition of a sample by analyzing the light emitted from excited atoms. In AES, atoms in a sample are excited to higher energy levels by thermal energy from high-temperature sources, such as plasma, arcs, or sparks. When these excited atoms return to lower energy states, they emit light at specific wavelengths characteristic of each element. The resulting atomic emission spectrum, which consists of...
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Atomic Emission Spectroscopy: Instrumentation01:22

Atomic Emission Spectroscopy: Instrumentation

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The instrumentation of atomic emission spectrometry (AES) involves various components, including atomization devices that convert samples into gas-phase atoms and ions. There are two main types of atomization devices: continuous and discrete atomizers.  Continuous atomizers, like plasmas and flames, introduce samples in a constant stream, while discrete atomizers inject individual samples using syringes or autosamplers. The most common discrete atomizer is the electrothermal atomizer.
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Electron Paramagnetic Resonance (EPR) Spectroscopy: Organic Radicals01:17

Electron Paramagnetic Resonance (EPR) Spectroscopy: Organic Radicals

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Ideally, an unpaired electron shows a single peak in the EPR spectrum due to the transition between the two spin energy states. However, coupling interactions can occur between the spins of the unpaired electron and any neighboring spin-active nuclei. This hyperfine coupling results in hyperfine splitting, where the EPR signal is split into multiplets. The signals split into 2nI + 1 peaks, where n is the number of equivalent nuclei and I is the nuclear spin. These splitting patterns provide...
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Angle-resolved Photoemission Spectroscopy At Ultra-low Temperatures
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一种高效的电子图谱法,用于从仅仅几次代中获取物体光谱.

Zhongbo Li1, Johannes Biskupek1, Martin Linck2

  • 1Electron Microscopy Group of Materials Science, University of Ulm, Ulm 89081, Germany.

Microscopy and microanalysis : the official journal of Microscopy Society of America, Microbeam Analysis Society, Microscopical Society of Canada
|March 20, 2024
PubMed
概括

我们开发了一种新的电子图谱法,可以有效地检索物体光谱. 这种方法通过处理透镜转移函数和衍射波来改善相位成像,即使数据有限.

关键词:
这是OSR的OSR.电子剂量的电子剂量对象频谱的对象频谱是什么?阶段重建重建的阶段重建.图形摄影 (ptychography) 是一种图形摄影技术.采样采样 采样采样

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科学领域:

  • 电子显微镜的电子显微镜
  • 材料科学是一种材料科学.
  • 计算机成像成像技术

背景情况:

  • 电子图像摄影是一种强大的高分辨率成像技术.
  • 电子图解现有的算法,如图解代引擎和非代方法,都有局限性.
  • 精确的相位检索对于详细的纳米分析至关重要.

研究的目的:

  • 为电子图解学提出一种新而高效的数学方法.
  • 克服现有的电子图谱算法的局限性.
  • 探索各种参数对重建相位图像的影响.

主要方法:

  • 引入了一种新的数学关系,与已建立的图解算法不同.
  • 该方法有效处理三个变量:镜头转移函数,物体光谱和衍射波.
  • 对象光谱和衍射波之间的代循环在很少的代中获取对象光谱,特别是在异常校正电子显微镜中.

主要成果:

  • 该对象频谱检索方法在计算和实验4D-STEM数据集上成功测试.
  • 该方法在重建物体光谱方面表现出了效率.
  • 研究了采样,剂量和照明孔径大小对重建相位图像的影响.

结论:

  • 本文所介绍的电子图谱法为相位检索提供了一个有效的替代方案.
  • 这种技术有可能提高纳米尺度成像的质量并减少对数据的要求.
  • 对参数影响的进一步探索可以为特定应用优化成像条件.