铁化物添加对软木木材的效果 纳米纤维稳定和碳化
Maxime Parot1, Denis Rodrigue2, Tatjana Stevanovic1
1Wood and Forest Science Department, Laval University, Quebec, QC G1V 0A6, Canada.
Polymers
|March 28, 2024
概括
将铁 (III) 化物 (FeCl3) 添加到软木中,可以提高纳米碳纤维的产量. FeCl3在稳定过程中提高了热稳定性,并在碳化后影响表面特性,产生高质量的碳纳米纤维.
科学领域:
- 材料科学 材料科学 材料科学
- 纳米技术纳米技术
- 化学工程是化学工程的重要组成部分.
背景情况:
- 软木有机溶解素是先进材料的可持续前体.
- 纳米碳纤维为各种应用提供独特的特性.
- 优化生产流程对于高效的材料合成至关重要.
研究的目的:
- 调查铁 (III) 化物 (FeCl3) 对软木纳米碳纤维生产的影响.
- 为了确定FeCl3对热稳定和碳化阶段的影响.
- 评估FeCl3对生产的碳纤维最终特性的影响.
主要方法:
- 准备了含有或不含有2%FeCl3的红素溶液.
- 电是用来生产素纳米纤维的.
- 福利埃变换红外光谱法 (FTIR) 和X射线光电子光谱法 (XPS) 用于分析.
- 用热重力测量分析 (TGA) 和扫描电子显微镜 (SEM) 来评估纤维特性.
主要成果:
- 在稳定过程中,添加FeCl3增加了素纤维的热电阻.
- 发现最佳稳定温度为250°C.
- 在气下在600°C下2小时碳化,产生了含有93%碳的纤维.
- SEM揭示了FeCl3.3生产的纤维的表面粗性.
结论:
- 添加FeCl3对柔软木材的纳米碳纤维产生积极影响.
- FeCl3增强了热稳定性,并影响了碳纤维的表面形态.
- 这些发现表明FeCl3作为优化素衍生碳纳米纤维合成的有益添加剂.
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