静态压力对超声波液相脱皮的几层石墨烯静态压力的作用
Hu Zong1, Minhui Gao1, Aziz Ul Hassan Mohsan2
1College of Chemical Engineering, Zhejiang University of Technology, Hangzhou 310014, China; Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences, Ningbo 315201, China.
Ultrasonics sonochemistry
|April 5, 2024
概括
这项研究引入了一个循环超声波系统,以改善石墨烯的生产. 施加静态压力提高了几层石墨烯的产量和质量,为可扩展的制造提供了潜力.
科学领域:
- 材料科学 材料科学 材料科学
- 纳米技术 纳米技术
- 化学工程是化学工程的重要组成部分.
背景情况:
- 超声波液相脱皮 (LPE) 是一种成本效益高的石墨烯生产方法.
- 对LPE的挑战包括低产量和延长的生产时间.
研究的目的:
- 开发一种改进的LPE方法,以提高石墨烯产量和质量.
- 为了研究静态压力对几层石墨烯生产的影响.
主要方法:
- 使用循环超声波系统对膨胀石墨 (EG) 进行脱皮.
- 在超声波过程中,在流体室内施加静态压力.
- 使用脱离离子水 (DIW) 作为溶剂,使用聚烯 (PVP) 作为分散剂.
主要成果:
- 平均横向尺寸为7微米的石墨烯泥和3.5层的石墨烯泥在40分钟内产生.
- 在离心后,单层和双层石墨烯的产量约为16%.
- 发现水静压有效地影响了几层石墨烯的侧面尺寸和层数.
结论:
- 带有静压的循环超声波系统有效地解决了LPE的局限性.
- 这种方法显示出大规模生产少层石墨烯的巨大潜力.
- 控制水静压是优化石墨烯特性的关键.
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