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在 ConsiGmaTM-25:第1部分颗粒组成中的双螺杆湿颗粒的控制概念的开发和应用:第1部分颗粒组成

Selma Celikovic1, Johannes Poms2, Johannes Khinast3

  • 1Research Center Pharmaceutical Engineering GmbH, Inffeldgasse 13/2, 8010 Graz, Austria; Institute of Automation and Control, Graz University of Technology, Inffeldgasse 21b, 8010 Graz, Austria.

International journal of pharmaceutics
|April 18, 2024
PubMed
概括

这项研究开发了用于制药连续制造的质量控制 (QbC) 算法. 该系统优化双螺丝湿颗粒,确保一致的颗粒组成,并在干扰时提供实时操作员支持.

关键词:
西格玛 (TM) - - 25个国家数字操作员助理数字操作员助理故障检测 检测故障检测颗粒组合 颗粒组合过程分析技术 (PAT) 是一种分析技术.过程控制 过程控制双螺丝湿颗粒制造的双螺丝制造

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Precipitation Processes01:12

Precipitation Processes

The experimental conditions in a gravimetric analysis should be optimized to maximize the particle size and purity of the obtained precipitate. Ideally, the concentration of the precipitating reagent should be low with effective stirring to maintain low relative supersaturation for the growth of large crystals. In homogeneous precipitation, the precipitant is slowly generated by a chemical reaction in the solution to avoid local reagent excesses. For example, urea decomposes gradually to...
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