对化Hydroxyapatite的正电子消灭寿命和光发光度测量之间的相关性
Hoda Atta1, Kamal R Mahmoud2, El Sayed I Salim3
1Physics Department, Faculty of Science, Kafrelsheikh University, Kafrelsheikh, 33516, Egypt. hoda_mera2014@sci.kfs.edu.eg.
Scientific reports
|May 6, 2024
概括
通过湿化学沉合成的Hydroxyapatite纳米颗粒表现出可调整的形态和光发光特性. 这些发现突显了它们在光疗中无毒的生物医学和光学应用的潜力.
科学领域:
- 生物材料科学 生物材料科学
- 纳米技术纳米技术
- 材料化学 材料化学
背景情况:
- 酸 (HAp) 具有稳定的化学特性和对骨的亲和力,使其适用于牙科,骨科和癌症治疗.
- 了解HAp在纳米尺度上的特性对于开发先进的生物医学设备至关重要.
研究的目的:
- 在600°C使用湿化学沉来合成和表征化酸 (HAp) 纳米颗粒.
- 研究pH值对HAp的结构,形态和光发光特性的影响.
主要方法:
- 湿化学沉,然后在600°C进行化.
- 使用X射线衍射 (XRD),拉曼光谱,SEM,TEM,FTIR,光发光 (PL),Zeta潜力和PALS进行表征.
- 分析晶体结构,大小,形态,缺陷和光学特性.
主要成果:
- HAp样本形成了六角结构,具有首选的 (002) 方向,晶体大小在16-25nm之间.
- 形态从纳米棒到纳米球和类似大米的结构,取决于pH值.
- 光发光显示出因缺陷而产生的蓝色和绿色发射峰值;Zeta电位在3.94mV至-2.95mV之间.
结论:
- 通过pH调整,可以控制HAp纳米颗粒的合成.
- 缺陷显著影响HAp.Ap的光发光特性.
- 合成的HAp纳米颗粒显示出对非有毒生物医学和光学设备的前景,特别是在光疗中.
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