一个宽带脉冲放大器用于 Joule 加热实验在钻石天细胞
Zachary M Geballe1, Joseph Lai1, Michael J Walter1
1Earth and Planets Laboratory, Carnegie Institution for Science, Washington, District of Columbia 20015, USA.
The Review of scientific instruments
|May 8, 2024
概括
新的电子设备增强了脉冲焦耳加热,用于使用钻石细胞在极端压力下研究金属. 这种强大的系统在高压条件下提高了热物理性质的测量精度.
科学领域:
- 材料科学 材料科学 材料科学
- 高压物理 高压物理
- 物理化学 物理化学
背景情况:
- 脉冲焦耳加热对于研究反应性金属的热物理性质是有效的.
- 集成脉冲加热与钻石天细胞使高压研究成为可能.
- 以前的设计由于主动传感设备而遭受损坏和测量错误.
研究的目的:
- 设计和描述用于钻石天电池中脉冲焦耳加热的新电子设备.
- 克服以前设计的局限性,专注于强度和精度.
- 为了能够在极端压力下精确测量金属的热物理性质.
主要方法:
- 开发一种新的脉冲放大器,使用高侧开关和被动电感应.
- 脉冲放大器与电流探针和钻石细胞的集成.
- 采用四点探头几何与两个电压探头连接到钻石细胞体的电阻测量.
主要成果:
- 新系统可以将金属电线 (直径550微米) 在几十到几百GPa的温度下加热到数千克尔文.
- 脉冲持续时间 (5μs10 ms) 和峰值电流 (0.2200 A) 在三个数量级上是独立可变的.
- 四点探头阻力测量显示,在整个脉冲持续时间内,0.1 Ω假样品的精度高于5%.
结论:
- 开发的电子设备为钻石天电池中脉冲焦耳加热提供了强大而准确的方法.
- 这一进步有助于研究在极端高压条件下材料的热物理性质.
- 该系统在脉冲参数和测量精度方面的多功能性为材料研究开辟了新的途径.
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