衰老对Ni-丰富NiTi合金相变和机械行为的影响
Jerzy Ratajski1, Błażej Bałasz2, Katarzyna Mydłowska1
1Department of Biomedical Engineering, Faculty of Mechanical and Power Engineering, Koszalin University of Technology (KUT), ul. Śniadeckich 2, 75-453 Koszalin, Poland.
Materials (Basel, Switzerland)
|May 25, 2024
概括
本研究探讨了异热老化如何影响增材制造的- (NiTi) 合金中的相变. 老化改变了转变类型和温度,较长的老化时间缩小了马氏体到奥氏体的过渡范围.
科学领域:
- 材料科学 材料科学 材料科学
- 金工业是金工业的一个方面.
- 添加剂制造 添加剂制造 添加剂制造
背景情况:
- - (NiTi) 合金是重要的形状记忆材料.
- 增材制造 (SLM) 为NiTi提供了新的加工途径.
- 同热老化是一种后加工技术,可以改变合金的特性.
研究的目的:
- 调查异热老化对SLM生产的NiTi合金 (51.7at.%Ni) 阶段转换的影响.
- 描述转换序列,温度和物理性质的变化.
- 为了将衰老时间与观察到的微观结构和特性修改相关联.
主要方法:
- 差分扫描热量计 (DSC) 用于分析相变序列和温度.
- 用X射线衍射 (XRD) 来确定相位组成.
- 硬度和扬模量测量以评估机械性能.
主要成果:
- 在500°C进行同热老化1-100小时,将冷却转换从一阶段变为两阶段.
- 加热转化 (马氏体到奥氏体) 仍然是一步,但发生在更高的温度下,老化加快.
- 老化显著缩小了加热转换温度范围,硬度和扬模块等机械性能受到影响.
结论:
- 异热老化是一种有效的方法来调整增材制造的NiTi合金的相变行为.
- 长时间的老化过程导致马氏体-奥斯岩的转化在一致的温度范围内发生,无论合金成分或制造方法如何.
- 这些发现为优化NiTi合金性能在需要特定形状记忆特征的应用中提供了洞察力.
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