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Updated: Jun 25, 2025

Utilization of Stop-flow Micro-tubing Reactors for the Development of Organic Transformations
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Utilization of Stop-flow Micro-tubing Reactors for the Development of Organic Transformations

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从不稳定的有机试剂中扩大C-糖化物合成的范围,使用流式微反应器

Hiromichi V Miyagishi1, Yusuke Kimuro2, Yosuke Ashikari1

  • 1Department of Chemistry, Graduate School of Science, Hokkaido University, Kita-10 Nishi-8 Kita-ku, Sapporo 060-0810, Japan.

Organic letters
|May 31, 2024
PubMed
概括

流式微反应器可以有效合成C-糖化物,这是多功能药物支架. 这种方法克服了传统合成的局限性,允许更高的温度和更广泛的基板范围,用于潜在的工业应用.

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A Scalable Balz-Schiemann Reaction Protocol in a Continuous Flow Reactor

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Real-time Monitoring of Reactions Performed Using Continuous-flow Processing: The Preparation of 3-Acetylcoumarin as an Example

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相关概念视频

Preparation of 1° Amines: Gabriel Synthesis01:28

Preparation of 1° Amines: Gabriel Synthesis

Direct alkylation is not a suitable method for synthesizing amines because it produces polyalkylated products. Gabriel synthesis is the most preferred method to exclusively make primary amines. The method uses phthalimide, which contains a protected form of nitrogen that participates in alkylation only once to predominantly give primary amines.
Strong bases like NaOH or KOH deprotonate the phthalimide to form the corresponding anion, which acts as a nucleophile. Further, the anion attacks an...
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