汉斯塔特 (HunStat) - - 一个简单,低成本的潜力计,用于分析和教育目的
Istvan Vamos1, Vilmos Kertesz2
1Lajos Petrik Vocational Chemistry School, Budapest, Hungary.
Analytical methods : advancing methods and applications
|June 11, 2024
概括
开发了一种低成本的DIY电压器,用于电化学分析. 这款紧型设备支持多种电压测量技术,非常适合教育和分析应用.
科学领域:
- 电化学 电化学 电化学
- 仪器化 仪器化 仪器化
- DIY科学 DIY科学 DIY科学
背景情况:
- 电位定位器对于电化学测量是必不可少的,但可能昂贵.
- 可访问的仪器对于扩大电化学研究和教育至关重要.
研究的目的:
- 开发一个低成本,用户友好的,DIY (DIY) 潜力机.
- 为分析和教育目的提供多功能电化学工具.
主要方法:
- 使用了一个Seeeduino XIAO微控制器,集成了数字对模拟 (D/A) 和模拟对数字 (A/D) 转换器.
- 实施了对循环电压测量 (CV),差异脉冲电压测量 (DPV) 和时频计 (CA) 的支持.
- 提供开放访问的设计文件,电路图,材料清单和软件 (Arduino草图,控制软件).
主要成果:
- 成功设计和制造了一种价格为15美元的紧电位器,输出电位范围为±1.65V.
- 开发了配套软件,方便参数操作和结果可视化.
- 该装置适用于各种电压测量技术.
结论:
- 开发的DIY电位器为电化学研究提供了具有成本效益和可访问性的解决方案.
- 这种仪器是强烈推用于教育环境和分析实验室寻找负担得起的仪器仪表.
相关概念视频
Potentiometry: Overview
2.0K
Potentiometry is an analytical technique that measures the potential difference between two electrodes in an electrochemical cell without drawing any significant current that could alter the solution's composition. This method employs an indicator electrode, which exchanges electrons with the analyte solution, and a reference electrode with a constant potential. Each electrode is immersed in a solution comprised of two half-cells. In a conventional setup, the reference electrode serves as...
2.0K
Controlled-Potential Coulometry: Electrolytic Methods
158
Controlled-potential coulometry, also known as potentiostatic coulometry, employs a three-electrode system in which the working electrode's potential is precisely regulated using a potentiostat. Platinum working electrodes are utilized for positive potentials, while mercury pool electrodes are favored for extremely negative potentials. The platinum counter electrode is separated from the analyte using a membrane or salt bridge to avoid interference in the analysis.
The chosen potential...
The chosen potential...
158
Potentiometry: Types of Electrodes
632
Reference electrodes serve as a stable reference point for potentiometric measurements, while indicator and working electrodes react to variations in the composition of a solution.
The Standard Hydrogen Electrode (SHE) is a widely used reference electrode that maintains zero potential across all temperatures. However, its need for a continuous hydrogen gas supply renders it impractical for everyday use.
An alternative to SHE is the Saturated Calomel Electrode (SCE). This electrode features an...
The Standard Hydrogen Electrode (SHE) is a widely used reference electrode that maintains zero potential across all temperatures. However, its need for a continuous hydrogen gas supply renders it impractical for everyday use.
An alternative to SHE is the Saturated Calomel Electrode (SCE). This electrode features an...
632
Voltammetry: Overview
1.7K
Voltammetry is an electroanalytical technique in which the current flowing through an electrochemical cell is measured as a function of applied potential, typically under conditions of concentration polarization. The technique provides valuable information about redox-active species, and the current response is plotted as a voltammogram.
A voltammetric cell uses three electrodes: a working electrode, a reference electrode, and an auxiliary electrode. The redox reactions occur in the working...
A voltammetric cell uses three electrodes: a working electrode, a reference electrode, and an auxiliary electrode. The redox reactions occur in the working...
1.7K
Controlled-Current Coulometry: Overview
198
Controlled current coulometry, also known as amperostatic coulometry, is a technique used in electrochemical analysis to measure the quantity of a substance through the controlled passage of current. It involves the application of a constant current to an electrochemical cell containing the analyte of interest. As the current flows through the cell, the analyte undergoes a redox reaction at the electrode surface, resulting in a charge transfer. By monitoring the time required for a certain...
198
Electrogravimetric Analysis: Overview
220
Electrogravimetric analysis measures the weight of an analyte deposited electrolytically onto a suitable working electrode. This method involves applying a potential to a pre-weighed electrode submerged in a solution, which results in the desired substance being deposited through reduction at the cathode or oxidation at the anode. The electrode's weight is recorded after deposition, and the difference in weight gives the analyte's weight in the solution.
To test the completeness of the...
To test the completeness of the...
220


