在天然和饮用水中分析微塑料的常规方法是通过与气色谱-质谱相结合的热解
Joan Dalmau-Soler1, M Rosa Boleda1, Silvia Lacorte2
1Aigües de Barcelona, Empresa Metropolitana de Gestió del Cicle Integral de l'Aigua, S.A., General Batet 1-7, 08028 Barcelona, Spain.
Journal of chromatography. A
|July 17, 2024
概括
一种新方法使用热解气色谱-质谱学准确测量饮用水中的微塑料 (MPs). 这种快速技术量化了MP,对于评估水安全和人类健康风险至关重要.
科学领域:
- 环境化学环境化学
- 分析化学 分析化学
- 水的质量 水的质量
背景情况:
- 微塑料 (MP) 在水生环境中普遍存在,引发了人们对人类健康影响的担忧.
- 标准化分析方法对于准确的饮用水MP测定至关重要.
研究的目的:
- 开发和验证一种简单,快速和定量方法,用于水中的MP分析.
- 为了确定各种水源中的MP度.
主要方法:
- 开发了一种使用 pyrolysis-gas chromatography-mass spectrometry (Py-GC-MS) 进行MP识别的方法.
- 评估方法性能,包括检测极限,线性,精度,准确性和不确定性.
- 通过 EUROQCHARM 实验室间练习验证了该方法.
主要成果:
- 通过Py-GC-MS方法在水样中成功确定了7种聚合物类型.
- 方法验证显示,5种测试的聚合物中的4种具有可接受的Z分数.
- 巴塞罗那水中的MP度从11.3μg/L到77.1μg/L不等.
结论:
- 开发的Py-GC-MS方法为饮用水中的MP分析提供了一个简单,定量和快速的方法.
- 这种方法有助于监测和管理人类饮用水中的MP污染.
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