对Cu-Mg铁化纳米颗粒的结构性,电磁性和光学性质的光
Sushen Chandra Devsharma1,2, Md Lutfor Rahman1, Md Jakir Hossain2
1Institute of Glass and Ceramic Research and Testing (IGCRT), Bangladesh Council of Scientific and Industrial Research (BCSIR), Dhanmondi, Dhaka-1205, Bangladesh.
Heliyon
|July 23, 2024
概括
用铜添加酸铁素纳米颗粒进行了合成和表征. 结果显示可调节的磁性和电性,表明传感器和微波设备的潜力.
科学领域:
- 材料科学 材料科学 材料科学
- 纳米技术纳米技术
- 固态物理 固态物理
背景情况:
- 铁酸盐 (MgFe2O4) 是一个有前途的材料,用于各种应用.
- 用过渡金属 (如铜) 进行兴奋剂可以改变其性能.
- 纳米材料由于其高表面积,提供了增强的特性.
研究的目的:
- 为了合成和特征铜合铁酸 (Mg1-xCuxFe2O4) 纳米材料.
- 研究铜度对结构性,磁性和电气性质的影响.
- 探索这些纳米材料的潜在应用.
主要方法:
- 索尔凝合成方法,然后在600°C下烧结.
- 使用X射线衍射 (XRD),扫描电子显微镜 (SEM),传输电子显微镜 (TEM),能量分散X射线光谱 (EDS),振动样本磁力测量 (VSM),紫外线可见光谱和阻抗分析进行表征.
- 分析结构参数,结晶体大小,晶格参数,磁性特性 (和磁化,强制性,保持性),带隙能量,介电性质和阻抗.
主要成果:
- 单相立方螺旋结构 (Fd3m空间组) 由XRD.证实.
- 结晶体大小在11-23纳米之间;格子参数随着Cu doping的增加而下降.
- 和磁化和强制性显示出度依赖的增强,分别达到28.96emu/gm和1102 Oe.
- 带间隙能量随着Cu含量增加而增加;介电性质表现出典型的费里特行为,在低频率下放松.
结论:
- 铜兴奋剂有效地改变了铁纳米材料的结构和磁性特性.
- 合成的Mg-Cu铁素纳米粒子表现出适合应用的可调节性质.
- 潜在的应用包括湿度传感器,气体传感器,微波设备和光催化剂.
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