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在系统中具有发光特性的玻璃陶材料 ZnO-B₂O₃-Nb₂O₅-Eu₂O₃

Lyubomir Aleksandrov¹, Aneliya Yordanova¹, Margarita Milanova¹

¹Institute of General and Inorganic Chemistry, Bulgarian Academy of Sciences, G. Bonchev, Str., bld. 11, 1113 Sofia, Bulgaria.

Molecules (Basel, Switzerland)

|August 10, 2024

概括

这项研究详细介绍了ZnO-B2O3-Nb2O3:Eu2O3玻璃陶的结晶和发光. 在经过25小时的热处理后,可以达到最佳的排放强度,这表明在光学材料中具有潜在的应用.

科学领域:

材料科学材料科学材料科学
固态化学固态化学
发光的光度是非常的低.

背景情况:

玻璃陶提供可调节的光学性能.
使用稀土元素,如欧 (Eu3+) 的兴奋剂可以增强发光.
了解结晶是优化玻璃陶性能的关键.

研究的目的:

为了研究50ZnO:47B2O3:3Nb2O3:0.5Eu2O3玻璃的结晶行为.
分析由此产生的玻璃陶的发光特性.
为了确定最佳的热处理以提高Eu3+排放.

主要方法:

差分扫描热量计 (DSC) 用于热分析.
用于相位识别和晶体结构分析的X射线衍射 (XRD).
传输电子显微镜 (TEM) 用于微观结构的研究.
光发光谱学用于评估光学特性.

主要成果:

证实了α-Zn3B2O6,β-Zn3B2O6和ZnNb2O6阶段的结晶.
欧离子成功地被纳入β-Zn3B2O6晶体相.
玻璃陶与原始玻璃相比,由于Eu3+离子不对称性增加,表现出增强的光发光.
在热处理25小时的样品中观察到最佳的排放强度.

结论:

热处理的持续时间显著影响ZnO-B2O3-Nb2O3:Eu2O3玻璃陶的结晶和发光特性.
将Eu3+纳入β-Zn3B2O6相增强发光,使这些材料对光学应用具有前景.
进一步的研究可以探索不同的组成和处理参数,以微调光学性能.

关键词:

这就是TEMEM.XRD XRD 在线观看玻璃陶的玻璃陶是什么意思发光效应的发光效应

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