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相关概念视频

Atomic Emission Spectroscopy: Instrumentation01:22

Atomic Emission Spectroscopy: Instrumentation

353
The instrumentation of atomic emission spectrometry (AES) involves various components, including atomization devices that convert samples into gas-phase atoms and ions. There are two main types of atomization devices: continuous and discrete atomizers.  Continuous atomizers, like plasmas and flames, introduce samples in a constant stream, while discrete atomizers inject individual samples using syringes or autosamplers. The most common discrete atomizer is the electrothermal atomizer.
353
Atomic Emission Spectroscopy: Overview01:20

Atomic Emission Spectroscopy: Overview

1.7K
Atomic emission spectroscopy (AES) is an analytical technique used to determine the elemental composition of a sample by analyzing the light emitted from excited atoms. In AES, atoms in a sample are excited to higher energy levels by thermal energy from high-temperature sources, such as plasma, arcs, or sparks. When these excited atoms return to lower energy states, they emit light at specific wavelengths characteristic of each element. The resulting atomic emission spectrum, which consists of...
1.7K
Atomic Emission Spectroscopy: Lab01:29

Atomic Emission Spectroscopy: Lab

152
AES is a powerful analytical technique, especially effective when used with plasma sources, producing abundant spectra in characteristic emission lines. The Inductively Coupled Plasma (ICP), in particular, yields superior quantitative analytical data due to its high stability, low noise, low background, and minimal interferences under optimal experimental conditions. However, newer air-operated microwave sources are emerging as promising alternatives that could be more cost-effective than...
152
Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation01:26

Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation

201
Inductively coupled plasma (ICP) is the common plasma source used in atomic emission spectroscopy (AES), a technique that detects and analyzes various elements in a sample. This method is often called inductively coupled plasma atomic emission spectroscopy (ICP-AES).
There are three main types of inductively coupled plasma atomic emission spectroscopy  (ICP-AES) instruments: sequential, simultaneous multichannel, and Fourier transform instruments, with the latter being less commonly used....
201
Inductively Coupled Plasma Atomic Emission Spectroscopy: Principle01:19

Inductively Coupled Plasma Atomic Emission Spectroscopy: Principle

556
Inductively coupled plasma (ICP) is the most widely used plasma source in atomic emission spectroscopy (AES), also known as Inductively Coupled Plasma Optical Emission Spectroscopy (ICP-OES). The ICP source, or torch, consists of three concentric quartz tubes with argon gas flowing through them. A spark from a Tesla coil initiates the ionization of argon, generating a high-temperature plasma.
The ions and electrons produced interact with the fluctuating magnetic field created by a water-cooled...
556
Atomic Fluorescence Spectroscopy01:29

Atomic Fluorescence Spectroscopy

258
Atomic fluorescence spectroscopy (AFS) is an analytical technique that involves the electronic transitions of atoms in a flame, furnace, or plasma being excited by electromagnetic (EM) radiation. When these atoms absorb energy, they become excited and subsequently release energy as they return to their original state. This emitted light, or "fluorescence," is observed at a right angle to the incident beam. Both absorption and emission processes transpire at distinct wavelengths, which...
258

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Single Molecule Fluorescence Microscopy on Planar Supported Bilayers
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Single Molecule Fluorescence Microscopy on Planar Supported Bilayers

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计算机模拟和建模发光放电光学辐射编码的光圈元素映射元素映射.

Harsshit Agrawaal1, Gerardo Gamez1

  • 1Texas Tech University, Department of Chemistry and Biochemistry, Lubbock, TX, 79409-41061, USA.

Analytica chimica acta
|August 18, 2024
PubMed
概括

一种新的方法,光放电光辐射编码孔径元素映射 (GOCAM),使得纳米级材料的快速元素映射. 这种技术大大缩短了采集时间,克服了先进材料分析当前方法的局限性.

科学领域:

  • 材料科学 材料科学 材料科学
  • 频谱学是一种光谱学.
  • 纳米技术纳米技术

背景情况:

  • 元素映射 (EM) 对于跨学科分析固体样本至关重要.
  • 现有的电磁技术,包括光放电光学发射光谱学 (GDOES) 与高光谱成像 (HSI) 相结合,由于采集时间长和样品消耗有限.
  • 需要更快的HSI来实现高通量GDOES用于纳米级材料分析.

研究的目的:

  • 为固体样本开发一种新的,快速的元素映射技术.
  • 解决当前EM方法中缓慢的获取时间和分辨率损失的局限性,特别是对于纳米材料.

主要方法:

  • 光放电的介绍 光辐射编码孔径元素映射 (GOCAM),一种使用压缩编码孔径光谱成像的技术.
  • 计算机模型模拟以优化编码的光圈参数 (元素大小,传导率) 以确保数据的准确性.
  • 对压缩感应重建算法的评估和比较,SeSCIGPU显示出卓越的性能.

主要成果:

  • 模拟表明,在较小的面罩元素尺寸和60%的传导率下,数据保证了最佳的数据保真度.
  • 在可靠性方面,SeSCIGPU的性能优于其他经过测试的重建算法 (TwIST,GAP-TV,SeSCICPU,ADMM-TV).
关键词:
编码的光圈孔口.压缩感应感应 压缩感应基本的绘制元素映射.发光放电光学发射光谱学 光学发射光谱学纳米材料是一种纳米材料.

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  • 该研究表明GOCAM的可行性用于单次暴露多元元素映射.
  • 结论:

    • GOCAM是一种可行的技术,用于快速元素测绘.
    • 开发的方法为未来的硬件开发提供了基础.
    • GOCAM有可能通过实现次秒多元元素映射来彻底改变纳米结构材料的表征.