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Updated: Jun 13, 2025

Low Pressure Vapor-assisted Solution Process for Tunable Band Gap Pinhole-free Methylammonium Lead Halide Perovskite Films
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Published on: September 8, 2017

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无金属矿固体溶液的溶剂辅助机械化学结晶 (H2dabco,H2hmta) NH4(BF4) 3

Jumpei Moriguchi1, Tomoe Koga2, Nao Tsunoji3

  • 1Graduate School of Sciences and Technology for Innovation, Yamaguchi University, Yoshida 1677-1, Yamaguchi, 753-8512, Japan. ryotsuna@yamaguchi-u.ac.jp.

Chemical communications (Cambridge, England)
|September 16, 2024
PubMed
概括

机械化学结晶的无金属矿固体溶液 ((d,h) -BF4) 呈现出取决于成分的分子动态. 在H2dabco2+中发生动态障碍,即使在塑性晶体相转变温度以下.

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The experimental conditions in a gravimetric analysis should be optimized to maximize the particle size and purity of the obtained precipitate. Ideally, the concentration of the precipitating reagent should be low with effective stirring to maintain low relative supersaturation for the growth of large crystals. In homogeneous precipitation, the precipitant is slowly generated by a chemical reaction in the solution to avoid local reagent excesses. For example, urea decomposes gradually to...
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