高温设置用于测量热电材料的霍尔系数和电导率
B Agrawal1, S Choudhary1, P K Sahu1
1Metallurgical Engineering and Materials Science, Indian Institute of Technology Bombay, Bombay 400076, India.
The Review of scientific instruments
|September 16, 2024
概括
一个新的实验设置可以同时测量高达700K的热电材料的霍尔系数和电导率. 这种多功能系统可确保高精度的热电性质的准确表征.
科学领域:
- 材料科学 材料科学 材料科学
- 固态物理 固态物理
- 实验物理实验物理学
背景情况:
- 热电 (TE) 材料的准确表征对于开发高效的能量转换装置至关重要.
- 同时测量霍尔系数 (RH) 和电导率 (σ) 提供了对 TE 材料中电荷载体行为的关键见解.
- 现有的方法可能在温度范围内有局限性,或需要单独测量,从而引入潜在的错误.
研究的目的:
- 开发和验证一种新的实验设置,用于同时测量 TE 标本的 RH 和 σ.
- 设计一个多功能样本持有器,容纳不同的TE样本尺寸,并促进多个TE属性测量.
- 确保 TE 材料表征开发的测量系统的高精度和可靠性.
主要方法:
- 使用范德保夫几何来同时测量霍尔系数 (RH) 和电导率 (σ).
- 设计了一个专门的样本持有器,以便轻松安装各种TE样本尺寸,并与其他TE测量 (Seebeck系数,热扩散率) 进行集成.
- 使用具有不同兴奋剂度的样和与校准设置相对应的验证导电数据,验证了仪器准确性.
主要成果:
- 在300700 K.的范围内实现了热电样本的同时RH和 σ测量.
- 证明了高精度,最大标准偏差为RH的±3%, σ的±0.5%.
- 验证了设置的准确性,显示与校准系统相比 σ 的偏差在 ± 3%,并确认适用于 n 型 (Mg2Sn) 和 p 型 (Mg3Sb2) TE 材料的适用性.
结论:
- 开发的实验设置为热电材料的同时RH和 σ测量提供了可靠和准确的方法.
- 多功能设计通过允许在同一样本上进行多种表征来最大限度地减少测量误差.
- 这一进步有助于更精确地评估热电材料的先进应用.
更多相关视频
相关概念视频
The Hall Effect
2.3K
Edwin H. Hall, in the year 1879, devised an experiment that could be used to identify the polarity of the predominant charge carriers in a conducting material. From a historical perspective, this experiment was the first to demonstrate that the charge carriers in most metals are negative.
2.3K
Thermal expansion and Thermal stress: Problem Solving
1.1K
San Francisco's Golden Gate Bridge is exposed to temperatures ranging from -15 °C to 40 °C. At its coldest, the main span of the bridge is 1275 m long. Assuming that the bridge is made entirely of steel, what is the change in its length between these temperatures?
To solve the problem, first, identify the known and unknown quantities. The initial length (L) of the bridge is 1275 m, the coefficient of linear expansion (α) for steel is 12 x 10-6/°C, and the change in...
To solve the problem, first, identify the known and unknown quantities. The initial length (L) of the bridge is 1275 m, the coefficient of linear expansion (α) for steel is 12 x 10-6/°C, and the change in...
1.1K
Calorimetry
2.9K
When objects at different temperatures are placed in contact with each other but isolated from everything else, they attain thermal equilibrium. A container that prevents heat transfer in or out is called a calorimeter, and the use of a calorimeter to make measurements is called calorimetry. Generally, these measurements involve heat or specific heat capacity. The term "calorimetry problem" is used for any problem where the specified objects are thermally isolated from their...
2.9K
Equipments Used to Measure Body Temperature
980
Body temperature can be assessed using various devices and measured in Celsius or Fahrenheit.
Glass-bulb Thermometer:
Glass-bulb thermometers are hollow glass tubes with a bulb tip containing liquid such as ethanol or mercury. Historically, glass bulb mercury thermometers were the standard device to measure body temperature. Today, mercury thermometers are prohibited in many countries due to the hazardous effects of mercury and the risk of exposure if the glass bulb breaks. In general,...
Glass-bulb Thermometer:
Glass-bulb thermometers are hollow glass tubes with a bulb tip containing liquid such as ethanol or mercury. Historically, glass bulb mercury thermometers were the standard device to measure body temperature. Today, mercury thermometers are prohibited in many countries due to the hazardous effects of mercury and the risk of exposure if the glass bulb breaks. In general,...
980


