从富含安东的提取物中去除多,使用4-维尼尔皮里丁交联共聚合物
Agnieszka Krzyszczak-Turczyn1, Marta Grochowicz2, Ilona Jonik1
1Department of Chemistry, Institute of Biological Sciences, Faculty of Medicine, Collegium Medicum, The John Paul II Catholic University of Lublin, Konstantynów 1J, 20-708 Lublin, Poland.
Food chemistry
|September 21, 2024
概括
新的微球吸附剂有效地从果提取物中捕获反素和黄类. 这些新型材料在先进分析之前对果实样本进行净化有前途,减少矩阵效应.
科学领域:
- 分析化学 分析化学
- 聚合物科学 聚合物科学
- 食品化学 食品化学
背景情况:
- 安西氨酸是具有健康益处的重要植物颜料.
- 纯化富含安东的提取物对于准确的分析至关重要.
- 现有的吸附剂可能无法有效地去除复杂的矩阵.
研究的目的:
- 评估新型4-乙烯基二烯的共聚物作为聚醇净化吸附剂.
- 评估聚烯4VP-co-TRIM) 和聚烯4VP-co-14DMB) 微球在捕获安托素和黄类物质方面的能力.
- 为了证明这些吸附剂在样本准备中对LC-MS/MS分析的有用性.
主要方法:
- 种子膨胀聚合合成多孔微球.
- 使用AFM,元素分析,SEM和吸附-溶解的特性.
- 通过光谱测量,HPLC-DAD和LC-MS/MS使用果提取物评估的多吸附.
主要成果:
- 合成的微球表现出永久的多孔结构.
- 新型吸附剂显示了比商业替代品更高的黄类吸附率.
- 观察到有效的安东基氨酸捕获,表明可能减少矩阵效应.
结论:
- 4 - - 乙烯基二烯的共聚物是净化素和黄类化合物的有效吸附剂.
- 这些微球为食品和植物提取物分析中的样本准备提供了有利的替代方案.
- 开发的吸附剂可以通过最小化矩阵干扰来提高LC-MS/MS分析的可靠性.
关键词:
4 - 基酸 (PubChem CID: 135) 的使用情况安托氨酸是一种安托氨酸.果果实是一种果.咖啡酸 (PubChem CID: 689043) 是一种咖啡酸.凯 (PubChem CID: 73160) 的一个例子.基酸 (PubChem CID: 1794427) 是一种可以使用的药物.分散固体相提取方法 分散固体相提取方法埃拉基酸 (PubChem CID: 5281855) 是一种酸.费鲁酸 (PubChem CID: 445858) 的使用情况黄类化合物 黄类化合物酸 (PubChem CID: 370) 的使用情况米瑞西丁 (PubChem CID: 5281672) 的使用情况聚合物材料是一种聚合物材料.奎尔丁 (PubChem CID: 5280343) 是一种可以使用的药物.鲁 (PubChem CID: 5280805) 已经成为一个常见问题.更多相关视频
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