使用微线结构进行X射线3D显微镜的放大校准
Yasushi Azuma1, Kazuhiro Kumagai1,2, Naoki Kunishima3
1National Metrology Institute of Japan (NMIJ), National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba Central 5, 1-1-1 Higashi, Tsukuba, Ibaraki 305-8565, Japan.
Microscopy (Oxford, England)
|September 24, 2024
概括
这项研究对量化测量进行了三维X射线显微镜 (3DXRM) 的校准. 使用扫描电子显微镜 (SEM) 评估线结构,获得了1.01的放大校准系数,使SI可追溯测量.
科学领域:
- 计量学 计量学 计量学
- 材料科学 材料科学 材料科学
- 图像技术技术的成像技术
背景情况:
- 三维X射线显微镜 (3DXRM) 是一种强大的非破坏性成像技术,用于亚微米尺度结构分析.
- 目前的3DXRM应用主要是观测性的,由于缺乏校准,限制了其在定量评估和质量控制中的使用.
- 精确的测量需要校准可追溯到国际单位系统 (SI).
研究的目的:
- 建立一个用于定量测量的3DXRM放大校准的方法.
- 为了验证3DXRM校准的原型标准样品 (线条结构).
- 评估为3DXRM创建一个SI可追溯的校准系统的可行性.
主要方法:
- 作为3DXRM放大校准的原型标准样本的制造线结构 (LS).
- 使用校准的横截面扫描电子显微镜 (SEM) 评估了LS的间隔.
- 将SEM和3DXRM评估结果进行比较,以确定放大校准因子.
主要成果:
- 根据SEM评估的LS间隔,为3DXRM确定了1.01的放大校准系数.
- 这些LS被验证为适合3DXRM校准的标准样本.
- 该研究证明了SI可追溯的3DXRM放大校准的可行路线.
结论:
- 开发的方法可以通过SI可追溯放大校准使用3DXRM进行定量测量.
- 这一进步显著提高了3DXRM在质量控制和计量学中的实用性.
- 这些发现为3DXRM在精密测量应用中的更广泛采用铺平了道路.
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