使用激光微加工和热机械分析仪在高温下对微型陶样品进行弹性模块测量
Zhao Zhang1, Hai Xiao2, Rajendra K Bordia1
1Department of Materials Science and Engineering, Clemson University, Clemson, SC 29634, USA.
Materials (Basel, Switzerland)
|September 28, 2024
概括
这项研究提出了一种新的方法,用于在高温下使用激光切割微光束测量陶柔性弹性模量. 该技术准确地描述了微型样本,验证了高级应用的陶材料特性.
科学领域:
- 材料科学 材料科学 材料科学
- 机械工程 机械工程
- 陶工程 陶工程 陶工程
背景情况:
- 在工程应用中,高温下精确测量陶机械性能至关重要.
- 传统方法可能不适合对散装陶的小,局部区域进行表征.
- 陶微机械性能的高温表征对于性能预测至关重要.
研究的目的:
- 展示一个精确的方法,以测量陶的柔性弹性模量在中间尺度.
- 为了使微型陶样品的高温表征.
- 为分析散装陶中局部材料特性提供准确的方法.
主要方法:
- 使用皮秒激光器进行精确的微光束切割 (约. 100微米×300微米的截面,~1厘米长) 来自散装陶.
- 使用热力学分析仪在各种温度下进行四点曲测试 (室温,500°C,800°C,1100°C).
- 通过将Al2O3和AlN的测量弹性模块与文献值进行比较,验证了该方法.
主要成果:
- 开发的方法准确地测量了在高温下陶微束的柔性弹性模量.
- 对高纯度氧化 (Al2O3) 和化 (AlN) 的实验结果显示,与报告的文献值的偏差不到5%.
- 证明了在散装陶中描述局部机械性能的可行性.
结论:
- 本文介绍了一种新的,准确和可靠的方法,用于确定微型陶样品的高温柔性弹性模量.
- 该技术允许在散装陶材料中对特定感兴趣的区域进行表征.
- 这些发现支持使用这种方法进行先进的材料分析和高温陶应用的质量控制.
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