开发用于水活动的化溶液的认证参考材料
Airui Zhang1, Haifeng Wang1, Xiao Li1
1National Institute of Metrology of China, Beijing, China.
Food chemistry
|November 4, 2024
概括
用于水活动 (a) 的认证参考材料是使用化溶液开发的. 这些材料确保了水活动计的准确校准,以确保食品安全和质量控制.
科学领域:
- 食品科学 食品科学 食品科学
- 分析化学 分析化学
- 计量学 计量学 计量学
背景情况:
- 水活动 (a) 对于评估食品的微生物稳定性,保质期和安全性至关重要.
- 基于电气湿度传感器的水活动表提供了方便的测量.
- 精确校准这些仪表对于可靠的结果至关重要.
研究的目的:
- 准备和认证化 (LiCl) 溶液作为水活动的参考材料.
- 建立可追溯和准确的标准,用于校准水活动表.
- 验证用于确定水活动的分析方法.
主要方法:
- 用于制备LiCl溶液的重力测量方法.
- 结合质量平衡和电位计定位以确定LiCl纯度.
- 德拜-赫克尔方程用于计算透系数 (φ).
- 使用已确定的物理化学原理计算经过认证的水活动值.
主要成果:
- 成功准备了两个用于水活动的认证参考材料 (CRM).
- 确定了具有不确定性 (U,k=2) 的认证值:0.250 ± 0.006和0.500 ± 0.007.
- 准备好的CRMs为水活动测量提供了准确的标准.
结论:
- 开发的LiCl CRMs适用于校准水活动表.
- 这些CRM可用于验证用于确定水活动的分析方法.
- 确保食品安全和质量评估的准确性和可靠性得到提高.
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