在空气大气中的氧化烤过程中聚酸的烧结行为:烤温度和K含量的影响
Jiangang Liu1, Lu Wang2, Guohuan Wu3
1College of Mechanical and Electrical Engineering, Wuyi University, Wuyishan 354300, China.
Molecules (Basel, Switzerland)
|November 9, 2024
概括
在化聚合物烤过程中,烧结会因高温和 (K) 含量而恶化. 减少这些因素可以有效地减少烧结,提高产品质量和炉子寿命.
科学领域:
- 金属学和材料科学 金属学和材料科学
- 化学工程是化学工程的重要组成部分.
- 矿物加工 矿物加工
背景情况:
- 在多炉炉中,在化聚酸氧化烤过程中,烧焦是关键问题.
- 这种现象会对产品质量和炉运行寿命产生负面影响.
研究的目的:
- 为了研究烤温度和 (K) 含量对化聚合物聚合物的影响.
- 确定有效的策略,以减轻氧化烤过程中的烧结.
主要方法:
- 在不同烤条件下对卜丁酸盐度的实验分析.
- 利用X射线衍射 (XRD),场辐射扫描电子显微镜与能量分散光谱 (FESEM-EDS) 以及相图进行数据分析.
主要成果:
- 烤温度的增加导致更高的质量损失和更严重的烧结.
- 高的K含量最初会增加质量损失,但会持续加剧烧结程度.
- 烧结产品呈现出含有MoO3,未氧化MoS2,SiO2和酸盐的复杂微结构,MoO3和酸盐是氨溶性的.
结论:
- 烧结是由局部温度升高和低点体的形成驱动的.
- 建议降低烤温度,特别是K含量,以减少化在乙烯酸缩加工中的作用.
相关概念视频
Alkali Metals
19.1K
Group 1 elements are soft and shiny metallic solids. They are malleable, ductile, and good conductors of heat and electricity. The melting points of the alkali metals are unusually low for metals and decrease going down the group, while the density increases going down the group with the exception of potassium (Table 1).
Table 1: Properties of the alkali metals
Table 1: Properties of the alkali metals
19.1K
Oxidation of Alkenes: Syn Dihydroxylation with Potassium Permanganate
11.0K
Alkenes can be dihydroxylated using potassium permanganate. The method encompasses the reaction of an alkene with a cold, dilute solution of potassium permanganate under basic conditions to form a cis-diol along with a brown precipitate of manganese dioxide.
11.0K
Sample Preparation for Analysis: Advanced Techniques
301
Accurate analysis of complex samples often requires advanced preparation techniques to achieve reliable and reproducible results. Samples containing inorganic or organic materials can be challenging to dissolve or decompose effectively. Standard sample preparation methods include acid digestion, fusion, dry ashing, and wet digestion.
Acid digestion with strong acids is commonly used to dissolve inorganic materials that are insoluble (do not dissolve) in water. This method can be useful for...
Acid digestion with strong acids is commonly used to dissolve inorganic materials that are insoluble (do not dissolve) in water. This method can be useful for...
301
Ionic Strength: Effects on Chemical Equilibria
1.4K
The addition of an inert ionic compound increases the solubility of a sparingly soluble salt. For example, adding potassium nitrate to a saturated solution of calcium sulfate significantly enhances the solubility of calcium sulfate. Le Châtelier's principle cannot predict this shift in the equilibrium. Instead, this could be explained in terms of changes in the effective concentration of the ions in solution in the presence of added inert salt.
In this solution, the primary...
In this solution, the primary...
1.4K
Radical Oxidation of Allylic and Benzylic Alcohols
1.9K
Activated manganese(IV) oxide can selectively oxidize allylic and benzylic alcohols via a radical intermediate mechanism. Primary allylic alcohols are oxidized to aldehydes, while secondary allylic alcohols yield ketones. The redox reaction of potassium permanganate with an Mn(II) salt such as manganese sulfate (under either alkaline or acidic conditions), followed by thorough drying, yields the oxidizing agent: activated MnO2. While MnO2 is insoluble in the solvents used for the reaction, the...
1.9K
Oxidation of Alkenes: Syn Dihydroxylation with Osmium Tetraoxide
9.9K
Alkenes are converted to 1,2-diols or glycols through a process called dihydroxylation. It involves the addition of two hydroxyl groups across the double bond with two different stereochemical approaches, namely anti and syn. Dihydroxylation using osmium tetroxide progresses with syn stereochemistry.
9.9K


