一个全面的热解气色谱/质谱分析,用于评估各种盐中的微塑料
Jihye Kwon1, Hyein Kim1, Muhammad Zain Siddiqui1
1Department of Energy System Engineering, Daegu University, Gyeongsan 38453, Republic of Korea.
Food chemistry
|December 3, 2024
概括
在食用盐中使用Py-GC/MS.量化了微塑料 (MPs). 海盐含有MPs度最高,导致人类暴露最大,其中PE,PP和PET是主要的聚合物.
科学领域:
- 环境化学环境化学
- 分析化学 分析化学
- 食品安全 食品安全
背景情况:
- 微塑料 (MP) 污染在食品中越来越令人担忧.
- 可食盐是MP摄入的潜在载体.
- 了解不同类型盐中的MP水平对于评估人类暴露至关重要.
研究的目的:
- 在各种可食盐中量化微塑料 (MP):海盐 (SS),深海盐 (DSS),岩盐 (RS) 和湖盐 (LS).
- 为了确定污染盐中存在的聚合物类型.
- 通过盐的消费来估计每年人类对MPs的暴露.
主要方法:
- 分析性热解气体染色学/质谱学 (Py-GC/MS) 用于MP量化.
- 使用20微米和1微米过器的两步过方法.
- 实施了质量控制措施和有效的方法,具有高线性和恢复率.
主要成果:
- 海盐 (SS) 的MP度最高 (584.5±204.4μg/kg),其次是岩盐 (RS) 和湖盐 (LS).
- 聚乙烯 (PE),聚烯 (PP) 和聚乙烯二甲 (PET) 是主要的MP类型,特别是在SS和RS中.
- 从包装材料中确认了MP污染,RS中发现的聚钢 (PS) 污染.
结论:
- 可食用盐,特别是海盐,是微塑料污染的重要来源.
- 人类接触MPs的程度因所摄取的盐类型而有很大差异.
- 这些发现强调了监测和减轻食品中MP污染的必要性.
相关概念视频
Gas Chromatography–Mass Spectrometry (GC–MS)
4.0K
Gas chromatography–mass spectrometry (GC–MS) is the combination of analytical techniques of gas chromatography and mass spectrometry in a single instrument for analyzing a mixture of compounds. The gas chromatograph separates the compounds in the mixture, and the mass spectrometer analyzes each compound separately to determine the molecular masses and molecular structures.
A gas chromatograph consists of a long, narrow capillary column with a polysiloxane coating on the inner wall....
A gas chromatograph consists of a long, narrow capillary column with a polysiloxane coating on the inner wall....
4.0K
Gas Chromatography: Types of Detectors-II
334
In gas chromatography, different detectors are employed to meet specific analytical needs. These detectors are often categorized based on their detection mechanisms and the types of compounds they are best suited to analyze. Thermal Conductivity Detectors (TCD), Flame Ionization Detectors (FID), and Electron Capture Detectors (ECD) represent common categories, each with unique operating principles and applications. However, beyond these, several other detectors are designed for more specialized...
334
Mass Spectrometry: Complex Analysis
716
Mass spectrometry is an important technique for the identification of pure compounds. However, it has some limitations for the analysis of complex mixtures, often due to excessive fragmentation making the spectrum too complicated to decipher. Mass spectrometry can be combined with suitable separation methods in sequence, forming hyphenated methods, which are useful in the analysis of complex mixtures.
GC–MS is a powerful hyphenated method commonly used in forensics and environmental...
GC–MS is a powerful hyphenated method commonly used in forensics and environmental...
716
Gas Chromatography: Introduction
1.4K
Gas chromatography (GC) is a technique for separating and analyzing volatile compounds in a sample. Its primary purpose is to identify and quantify components in complex mixtures, making it essential in fields such as environmental analysis, pharmaceuticals, and petrochemicals. GC is also called vapor-phase chromatography (VPC) or gas-liquid partition chromatography (GLPC).
In GC, a sample is vaporized and mixed with an inert carrier gas (the mobile phase), which transports it through a...
In GC, a sample is vaporized and mixed with an inert carrier gas (the mobile phase), which transports it through a...
1.4K


