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Atomic Absorption Spectroscopy: Atomization Methods01:25

Atomic Absorption Spectroscopy: Atomization Methods

372
Atomic Absorption Spectroscopy (AAS) atomizes samples through flame atomization or electrothermal atomization. Flame atomization typically involves a nebulizer and spray chamber assembly to combine the sample with a fuel–oxidant mixture, creating a fine aerosol mist that enters a burner. Typically, the fuel and oxidant are combined in an approximately stoichiometric ratio. However, for atoms that are easily oxidized, a fuel-rich mixture may be more advantageous. Only about 5% of the...
372
Atomic Emission Spectroscopy: Instrumentation01:22

Atomic Emission Spectroscopy: Instrumentation

338
The instrumentation of atomic emission spectrometry (AES) involves various components, including atomization devices that convert samples into gas-phase atoms and ions. There are two main types of atomization devices: continuous and discrete atomizers.  Continuous atomizers, like plasmas and flames, introduce samples in a constant stream, while discrete atomizers inject individual samples using syringes or autosamplers. The most common discrete atomizer is the electrothermal atomizer.
338

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Updated: Jun 5, 2025

Calibrated Passive Sampling - Multi-plot Field Measurements of NH3 Emissions with a Combination of Dynamic Tube Method and Passive Samplers
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描述动态大气生成系统的性能,用于分析方法的开发.

Amos Doepke1, Robert P Streicher1, Peter B Shaw1

  • 1Health Effects Laboratory Division, Chemical and Biological Monitoring Branch, Centers for Disease Control and Prevention, National Institute for Occupational Safety and Health, Cincinnati, Ohio.

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|December 4, 2024
PubMed
概括
此摘要是机器生成的。

这项研究评估了工作场所大气中的挥发性有机化合物 (VOC) 采样变异性. 随着度和挥发性有机化合物混合物的降低,变异性增加,为未来的采样方法评估提供了基线.

关键词:
空气采样采样空气采样这是一种VOC,可挥发性化合物.子皮木炭木炭样本变异性的样本变异性.挥发性有机化合物 挥发性有机化合物

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科学领域:

  • 工业卫生 工业卫生
  • 分析化学 分析化学
  • 环境科学 环境科学

背景情况:

  • 开发和验证工作场所大气中的挥发性有机化合物 (VOC) 采样方法通常依赖于实验室产生的大气.
  • 了解采样方法的变化和偏差对于准确的工作场所空气质量评估至关重要.

研究的目的:

  • 为了评估用于VOC采样的动态大气生成系统的样本变异性.
  • 为了描述在活性子皮木炭上收集的VOC样本的偏差和变异性.

主要方法:

  • 利用动态大气生成系统来创建受控的实验室大气.
  • 产生的大气包含纯净的n-heptane和VOC混合物.
  • 收集了活性子皮木炭的样本进行分析.

主要成果:

  • 估计的采样变化率从纯n-heptane的2%到10 VOC混合物的成分的12%.
  • 观察到较低度的VOC样本的样本变异性增加.
  • 与单个成分大气相比,VOC混合物的变异性更高.

结论:

  • 该研究为评估低度和混合VOC环境中的VOC采样性能提供了基线.
  • 结果突出了度和混合物复杂度对采样变异性的影响.
  • 结果对于提高工作场所空气监测VOC的准确性至关重要.