食品认证变得绿色:方法优化原产地歧视果使用果汁和ICP-MS
Marie-Sophie Müller1, Marie Oest1, Sandra Scheffler1
1Hamburg School of Food Science, Institute of Food Chemistry, University of Hamburg, Grindelallee 117, 20146 Hamburg, Germany.
Foods (Basel, Switzerland)
|December 17, 2024
概括
优化果汁的感应合等离子体质谱 (ICP-MS) 分析通过消除冷干燥,显著减少二氧化碳排放. 这种方法可以准确地确定果的原产地,区分欧洲,非欧洲和德国的区域来源.
科学领域:
- 食品科学 食品科学 食品科学
- 分析化学 分析化学
- 环境科学 环境科学
背景情况:
- 果在全球范围内具有重要意义,在德国消费量很高,但国内果价格较高,鼓励用外国产品造.
- 进口果由于运输和分析而带来更大的碳足迹,这在气候变化问题中带来了挑战.
- 准确的原产地确定对于消费者信任和解决与果供应链相关的环境影响至关重要.
研究的目的:
- 优化样品准备用于果汁的诱导合等离子体质谱 (ICP-MS) 分析,减少其碳足迹.
- 开发和验证一个ICP-MS方法,以准确区分果的原产地.
- 评估优化分析方法对环境的好处.
主要方法:
- 通过删除冷干燥步骤,优化了ICP-MS的样本准备,减少了约97%的二氧化碳排放.
- 优化的ICP-MS方法用于分析来自七个国家的272个果汁样本.
- 创建了统计模型来确定果汁样本的来源.
主要成果:
- 优化的ICP-MS方法成功地以高准确度区分了果的起源.
- 欧洲果与非欧洲果的区分精度为90.9%±2.4%.
- 德国的果与其他国家差异化准确度为83.2%±1.4%,区域差异化 (南北) 准确度为92.3%±5.4%.
结论:
- 优化的ICP-MS方法,消除了冷干燥的需要,对于确定果汁中的果原产地非常有效.
- 这种精简的分析方法显著降低了与果分析相关的碳足迹.
- 该方法为验证果原产地提供了可靠的工具,支持食品行业的公平贸易和环境可持续性.
相关概念视频
Inductively Coupled Plasma–Mass Spectrometry (ICP–MS): Overview
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In inductively coupled plasma–mass spectrometry (ICP–MS), an inductively coupled plasma (ICP) torch is used as an atomizer and ionizer. Solid samples are dissolved and volatilized before being introduced into the high-temperature argon plasma, while solution samples are nebulized and passed through the high-temperature argon plasma. Plasma dissociates the analytes and ionizes their component atoms to form a mixture of positive ions and molecular species. The positive ions are then...
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Inductively Coupled Plasma-Mass Spectrometry (ICP-MS): Interferences
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Inductively coupled plasma–mass spectrometry (ICP–MS) is a highly selective and sensitive technique for accurate elemental analysis. Though the analysis of ICP–MS mass spectra is comparatively straightforward, it is affected by spectroscopic and non-spectroscopic interferences. Spectroscopic interferences arise when the plasma contains ionic species with an m/z value the same as the analyte ion. Spectroscopic interference can be categorized as isobaric, polyatomic ions, and...
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