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Atomic Absorption Spectroscopy: Atomization Methods01:25

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Atomic Absorption Spectroscopy (AAS) atomizes samples through flame atomization or electrothermal atomization. Flame atomization typically involves a nebulizer and spray chamber assembly to combine the sample with a fuel–oxidant mixture, creating a fine aerosol mist that enters a burner. Typically, the fuel and oxidant are combined in an approximately stoichiometric ratio. However, for atoms that are easily oxidized, a fuel-rich mixture may be more advantageous. Only about 5% of the aerosol...

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在低床温度下激光烧结聚合物粉末的新加工方法.

Lanti Yang1, Hao Gu2, Zahir Bashir3

  • 1SABIC Analytical Science Europe, Corporate T&I, Plasticslaan 1, 4612 PX Bergen op Zoom, The Netherlands.

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概括

一种新型膜可以防止在较低床温度下激光烧结 (LS) 聚乙烯二甲 (PET) 等高性聚合物的部分扭曲. 这项创新使得150°C的PET能够成功打印,减少卷曲和曲面.

关键词:
在PA12中,PA12是PA12.在这里,PET是PET.添加剂制造 添加剂制造 添加剂制造激光烧结是一种激光烧结.低床位温度 床位温度低粉末 粉末 粉末 粉末

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科学领域:

  • 添加剂制造 添加剂制造 添加剂制造
  • 材料科学 材料科学 材料科学

背景情况:

  • 目前的激光烧结 (LS) 机器仅限于200°C的床温度,限制了像聚乙烯四甲酸盐 (PET) 这样的高性聚合物的使用.
  • 在LS的低床温度导致显著的部分扭曲 (卷曲和曲面) 由于结晶诱导的收缩.

研究的目的:

  • 在降低床温度下引入一种用于激光烧结 (LS) 高聚合物的新方法.
  • 为了克服LS中的部分扭曲问题,使用现场打印的片.

主要方法:

  • 开发了一种灵活的,70微米厚的膜,在现场打印.
  • 利用膜提供摩擦约束,防止LS期间卷曲和扭曲.
  • 在显著降低的床温度下成功打印了聚乙烯二甲 (PET) 和聚胺12 (PA12).

主要成果:

  • 在150°C的温度下成功打印PET零件,比标准工艺减少80°C,没有机器停机.
  • 在现场的膜有效地减轻了卷曲和曲面,这些问题通常在低床温度下遇到.
  • 对聚胺12 (PA12) 印刷的潜在好处,包括减少粉末降解和能源消耗.

结论:

  • 在现场打印的膜是一种有效的解决方案,可以实现像PET这样具有挑战性的高分子的低温激光烧结 (LS).
  • 这种方法比传统方法有了显著的进步,使用的是薄薄的可拆卸薄膜,而不是重的固定板.
  • 这种技术有望在增材制造中得到更广泛的应用,改善材料加工和能源效率.