对耐火高合金的热软化测量
Ottó K Temesi1,2, Albert Karacs3, Nguyen Q Chinh2
1H-ION Kft., Konkoly-Thege Miklós út 29.-33., H-1121 Budapest, Hungary.
Materials (Basel, Switzerland)
|December 17, 2024
概括
新的自制设备测量了高达1100°C的热膨胀和缩深度. 该系统使得研究全热相转换和材料热软化成为可能,这对于金属和高合金至关重要.
科学领域:
- 材料科学与工程 材料科学与工程
- 物理金学 物理金学
- 高温材料的特性 高温材料的特性
背景情况:
- 在高温下精确测量热力学性能对于理解材料的行为至关重要.
- 现有的1000°C以上同时进行热膨胀和缩测量的方法有限.
- 描述热软化和相位转换对于设计高温应用是必不可少的.
研究的目的:
- 介绍新型自制设备,用于测量高达1100°C的热膨胀和隙深度.
- 为了研究使用度计模式的全方位相位转换.
- 开发一种方法来量化隙深度作为温度的函数 (ID,T) 并测试一种新的热软化表达式.
主要方法:
- 开发一种双模式仪器,能够进行扩度测量和洛克韦尔型硬度测试.
- 使用平坦的入器进行热膨胀和尖的入器进行入深度测量.
- 采用差分方法,从高负荷曲线中减去低负荷位移曲线,以隔离隙深度.
主要成果:
- 该设备成功地测量了高达1100°C的热膨胀和缩深度.
- 可以在度仪模式下观察到全方位相变换.
- 观察并量化了明显的热软化行为,包括由于缩主导的明显收缩.
结论:
- 开发的自制设备为高温热力学表征提供了一个多功能平台.
- 作为温度的函数来确定内深度的新方法对于研究热软化是有效的.
- 这些发现为在高温下改进纯金属和耐火高合金 (HEAs) 的建模铺平了道路.
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