大量填充复合材料的网络完整性:热稳定性,固化后硬度的发展和酸性软化
Mohammed Aldhafyan1,2, Abdel-Basit Al-Odayni2, Waseem Sharaf Saeed2
1Restorative Dental Sciences Department, College of Dentistry, King Saud University.
Dental materials journal
|February 16, 2025
概括
这项研究表明,酸性软化显著降低了散装复合材料的硬度. 酸暴露后硬度下降可以间接评估复合材料.
科学领域:
- 牙科材料科学 牙科材料科学
- 聚合物化学 聚合物化学
- 生物材料是一种生物材料.
背景情况:
- 大量填充复合材料提供临床优势,但它们在口腔条件下的网络完整性需要进一步研究.
- 在口腔中常见的酸性环境可能会损害牙修复材料的机械性能.
- 了解散装复合材料对酸暴露的反应对于预测其临床寿命至关重要.
研究的目的:
- 在酸性软化后评估六种散装复合材料的热稳定性和上下硬度比.
- 为了将网络完整性与质量损失的初始最大速率温度 (IRT) 相关联.
- 建立酸性侵蚀硬度发展作为评估网络完整性的方法.
主要方法:
- 六个批量填充复合材料被制造成磁盘样本并进行光固化.
- 维克斯硬度是在固化后立即测量 (VH0),在24小时干燥储存后 (VHdry) 和在37°C的24小时酸性储存后 (VHacidic).
- 在酸性软化后的相对硬度下降 (VH_RD) 与初始最大速率温度 (IRT) 相比较.
主要成果:
- 维克斯硬度在干燥储存后显著增加,但与初始硬度相比,在酸性储存后显著下降.
- 上面表面的相对硬度下降 (VH_RD) 在测试的复合材料中差异很大,从16.62%到62.84%不等.
- 在IRT和VH_RD之间观察到负相关性,这表明IRT可以间接估计网络完整性.
结论:
- 酸性软化显著影响散装复合材料的硬度,降低它们的网络完整性.
- 最初的最大速率温度 (IRT) 显示了作为散装复合材料抵抗酸性降解的间接指标的潜力.
- 酸侵蚀硬度的发展可以作为一种可行的方法来评估散装复合材料的网络完整性.
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