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Updated: May 15, 2025

An Inexpensive Adaptation of a Commercial Microwave Reactor for Solid Phase Peptide Synthesis
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An Inexpensive Adaptation of a Commercial Microwave Reactor for Solid Phase Peptide Synthesis

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快速高效的微波辅助固体相合成Na3V2(PO4) 2F3以及对合成过程的探索

Fa He1, Jiyang Kang1, Ruoyang Wang1

  • 1School of Chemical Engineering, Sichuan University, Chengdu, 610065, China. zhenguowu@scu.edu.cn.

Chemical communications (Cambridge, England)
|April 7, 2025
PubMed
概括

我们开发了一种用于化 (NVPF) 阴极的快速微波辅助合成. 这种节能方法可以为先进的储能应用提供高性能材料.

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Development of a Backbone Cyclic Peptide Library as Potential Antiparasitic Therapeutics Using Microwave Irradiation08:48

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Protocol for the Solid-phase Synthesis of Oligomers of RNA Containing a 2'-O-thiophenylmethyl Modification and Characterization via Circular Dichroism11:37

Protocol for the Solid-phase Synthesis of Oligomers of RNA Containing a 2'-O-thiophenylmethyl Modification and Characterization via Circular Dichroism

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Preparation of 1° Amines: Gabriel Synthesis01:28

Preparation of 1° Amines: Gabriel Synthesis

Direct alkylation is not a suitable method for synthesizing amines because it produces polyalkylated products. Gabriel synthesis is the most preferred method to exclusively make primary amines. The method uses phthalimide, which contains a protected form of nitrogen that participates in alkylation only once to predominantly give primary amines.
Strong bases like NaOH or KOH deprotonate the phthalimide to form the corresponding anion, which acts as a nucleophile. Further, the anion attacks an...
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