化温度对聚乙烯糖醇稳定铁酸盐纳米颗粒的结构和磁性性能的影响
Samreen Zahra1, Uzma Naz2, Misbah Irshad2
1Mineral Processing Research Centre, Pakistan Council of Scientific and Industrial Research Laboratories Complex, Ferozepur Road, Lahore, 54600, Pakistan. samreenzahra68@hotmail.com.
BMC chemistry
|April 21, 2025
概括
纳米晶铁酸盐 (NiFe2O4) 是通过sol-gel方法合成的. 聚烯糖醇稳定了纳米颗粒,减少了聚合,产生了适合磁性存储设备的结构.
科学领域:
- 材料科学 材料科学 材料科学
- 纳米技术 纳米技术
- 固态化学 固态化学
背景情况:
- 铁 (NiFe2O4) 纳米颗粒通过水性sol-gel路径合成.
- 使用的酸和铁酸前体与水性乙醇和聚烯糖醇.
- 化温度在500°C至900°C之间进行,以研究性能变化.
研究的目的:
- 为了研究烧温度对铁酸盐纳米粒子特性的影响.
- 评估聚乙烯甘醇作为稳定剂的作用.
- 描述合成纳米粒子的结构和磁性属性.
主要方法:
- 使用酸和铁酸进行sol-gel合成.
- 在500°C至900°C的温度下进行化.
- 使用X射线衍射,红外光谱,热重力测量,FESEM和VSM进行表征.
主要成果:
- 形成具有立方螺旋结构的单相铁酸盐.
- 纳米粒子呈现出不规则的形状,尺寸在10-20纳米之间,随机分布形成聚合物.
- 聚烯糖醇有效地减少了初始纳米粒子聚合.
结论:
- 化温度影响了纳米粒子聚合,在900°C时产生了分散的结构.
- 铁纳米颗粒表现出高强制性,表明它们适合用于磁性存储和设备.
- 聚乙烯甘醇是控制纳米粒子形态和防止过度聚合的关键剂.
关键词:
场辐射扫描电子显微镜红外光谱法 红外光谱法 红外光谱法尼克尔铁酸盐是什么意思索尔格尔 (Solgel) 是一个非常好的解决方案.热重力测量是一种热重力测量.振动样品磁力测量振动样品磁力测量X射线衍射法X射线衍射法更多相关视频
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