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增强的DMA测试程序来测量以环氧为基础的成型化合物的粘弹性特性:多个振荡应变幅度和单调负荷
Sukrut Prashant Phansalkar1, Roshith Mittakolu1, Bongtae Han1
1Department of Mechanical Engineering, University of Maryland, College Park, MD 20742, USA.
Micromachines
|April 26, 2025
概括
这项研究引入了一种先进的动态机械分析 (DMA) 程序,用于测试高度填充的热,提高模量测量精度. 该方法可确保对像环氧成型化合物 (EMC) 等材料的可靠粘弹性性能数据.
科学领域:
- 材料科学 材料科学 材料科学
- 聚合物化学 聚合物化学
- 机械工程 机械工程
背景情况:
- 动态机械分析 (DMA) 对于半导体工业中热固聚合物的表征至关重要.
- 测试高度填充的热聚合物,如环氧成型化合物 (EMC),由于温度范围内的显著模量变化,提出了挑战.
- 现有的DMA方法可能会在这些材料所需的广泛动态范围方面扎.
研究的目的:
- 提出一种先进的DMA程序,用于准确测量高填充热的粘弹性特性.
- 为了应对像EMC这样的材料在DMA测试期间的大模量变化所带来的挑战.
- 提高主曲线构造和材料建模的可靠性.
主要方法:
- 利用不同的振荡应变幅度来保持一致的应力幅度变化.
- 在极端温度下进行单调测试,以确定玻璃和平衡模块.
- 构建放松模量主曲线并验证概括的麦克斯韦模型常量.
主要成果:
- 提议的先进的DMA程序有效地管理高填充热聚体的大模量变化.
- 准确确定玻璃和平衡模块有助于精确的主曲线构造.
- 使用放松模量主曲线的虚拟测试验证了通用麦克斯韦模型的准确性.
结论:
- 先进的DMA程序为表征具有挑战性的热固化聚合物提供了强大的解决方案.
- 这种方法提高了粘弹性属性确定和材料建模的准确性.
- 这些发现对于需要在苛刻环境中精确预测材料行为的应用具有重要意义.
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