使用高分辨率连续源石墨炉原子吸收光谱学直接固体分析对狗和猫零食中的Pb,Ni和Fe的顺序和同时确定
Nicole Evelyn de J Santos1, Rafael R Francisco1, Leandro Kolling2
1Universidade Federal da Bahia, Instituto de Química, Departamento de Química Analítica, Campus Universitário de Ondina, 40170-115, Salvador, Bahia, Brazil.
Talanta
|June 8, 2025
概括
一种新的分析方法使用直接固体分析和HR-CS GF AAS准确测量,和铁在物食品中的含量. 这种可靠的技术适用于物食安全的常规质量控制.
科学领域:
- 分析化学 分析化学
- 环境科学 环境科学
- 食品科学 食品科学 食品科学
背景情况:
- 物食品安全对于动物健康至关重要.
- 准确量化物食品中的重金属对于质量控制至关重要.
- 现有的分析方法可能需要复杂的样本准备.
研究的目的:
- 优化和验证一种直接固体分析方法,用于确定狗和猫的 (Pb), (Ni) 和铁 (Fe) 的含量.
- 确定方法的可靠性和适用于常规质量控制的适用性.
- 评估商业物处理样本中Pb,Ni和Fe的度.
主要方法:
- 直接固体分析与高分辨率连续源石墨炉原子吸收光谱学 (HR-CS GF AAS) 相结合.
- 优化石墨炉温度程序用于热解和原子化.
- 在217.001nm,232.003nm和232.036nm分别检测Pb,Ni和Fe的波长选择.
主要成果:
- 在800°C的最佳化热解和在1600°C (Pb) 或2500°C (Ni,Fe) 的原子化.
- 已达到0.33毫克公斤-1 (Pb),0.40毫克公斤-1 (Ni) 和1.4毫克公斤-1 (Fe) 的量化极限 (LoQ).
- 物食品中的度在0.9-2.9毫克公斤-1 (Pb),0.5-2.5毫克公斤-1 (Ni) 和121-617毫克公斤-1 (Fe) 之间.
结论:
- 开发的HR-CS GF AAS方法是有效和可靠的,用于直接确定物食品中的Pb,Ni和Fe.
- 该方法的准确性和精确性使其适用于例行质量控制和确保物食安全.
- 0.73的AGREE度量得分表明该方法的总体一致性和适用性良好.
关键词:
猫 猫 猫 猫 猫 猫 猫直接样本分析 直接样本分析狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗狗人权高官-CS GF AAS AAS 在零食 小吃 零食微量元素中的微量元素.更多相关视频
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