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Updated: Sep 17, 2025

Line Shape Analysis of Dynamic NMR Spectra for Characterizing Coordination Sphere Rearrangements at a Chiral Rhenium Polyhydride Complex
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Published on: July 27, 2022

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DOSY 在可变温度下进行NMR实验. 对可靠结果的最佳条件进行彻底分析

Israel Macho-Ávila1,2, Gabriel González-Ferrer1, Pablo Ballester1,3

  • 1Institut Català d'Investigació Química (ICIQ-CERCA), The Barcelona Institute of Science and Technology (BIST), Tarragona, Spain.

Magnetic resonance in chemistry : MRC
|July 2, 2025
PubMed
概括

本研究介绍了使用标准NMR设备在可变温度下进行多核扩散有序光谱 (DOSY) 的简单协议. 该方法通过优化实验条件和使用先进的脉冲序列来减轻对流效应,确保可靠的数据.

关键词:
19F 19F 19F 19F 19F 19F 19F 19F 19F 19F 19F 19F 19F 19F 19F一个小时 1H 1H31P 31P 31P 31P 31P 31P 31P 31P 31P 31P 31P 31P这是一个 DOSY 文件.这是NMR的NMR.电流对流是指对流的对流.脱的脱方式脉冲程序是一个脉冲程序.温度变量的温度变量.

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