通过EBSD对合金中的α相变体进行表征:了解颜色索引的挑战
1Centre for Additive Manufacturing, School of Engineering, RMIT University, Melbourne, VIC 3000, Australia.
电子反射散射衍射 (EBSD) 逆极图 (IPF) 地图可以由于颜色重叠而掩盖合金相变种. 这项研究澄清了阿尔法变体的EBSD染色,有助于准确的微观结构分析和材料设计.
科学领域:
- 材料科学 材料科学 材料科学
- 金工业是一种金工业.
- 晶体学 晶体学是指结晶学.
背景情况:
- 用反极形图 (IPF) 地图进行电子逆散射衍射 (EBSD) 对于可视化合金中的粒度方向至关重要.
- 在IPF地图中,由于颜色重叠,识别由Burgers定向关系支配的从beta转换到alpha转换的十二个alpha相变异是具有挑战性的.
研究的目的:
- 系统地研究EBSD IPF X,Y和Z地图中的α相变异的颜色.
- 解释IPF地图中多个变体的相似颜色背后的原因.
- 为了将IPF地图颜色分布与滑动系统的施密德因子相关联.
主要方法:
- 使用Ti-6Al-2Sn-4Zr-2Mo合金样本,通过激光导向能量沉积来制造.
- 分析了先前β粒及其α相变体的方向,使用汉堡的方向关系.
- 探索了IPF地图颜色分布与Schmid因子之间的关系,用于基底,镜和金字塔滑动.
主要成果:
- 展示了为什么多个α相变体在IPF地图中表现出类似的颜色.
- 提供了基于颜色分布和施密德因子的滑动系统和变形行为激活的见解.
- 澄清了IPF地图中阿尔法相变异的表示,解决了解释模两可的问题.
结论:
- 建立了一个框架,使用EBSD准确地对合金进行微结构性表征.
- 突出了IPF地图基于颜色的分析用于区分alpha变异的局限性.
- 强调需要补充技术来克服EBSD颜色限制,以改善材料设计.
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