超高温真空探测器用于电气和热量测量
Laurent Jalabert1,2, Jose Ordonez-Miranda1,2,3, Yunhui Wu2
1LIMMS, CNRS-IIS IRL 2820, The University of Tokyo, Tokyo 153-8505, Japan.
The Review of scientific instruments
|August 25, 2025
概括
我们开发了一个超高温真空探测站 (UHT-VPS),用于精确测量高达1150K的材料性质.
科学领域:
- 材料科学
- 热分析
- 电气特性
背景情况:
- 对于先进的应用来说,精确的材料特性在高温下至关重要.
- 现有的方法在极端条件下经常面临同时进行电和热测量的局限性.
研究的目的:
- 开发和验证一个超高温真空探测站 (UHT-VPS),用于同时测量电气和热性能.
- 展示该系统在测量大量蓝宝石和薄膜微电阻方面的能力.
主要方法:
- 在真空环境中使用来自碳化加热器的热辐射加热的无接触样本持有器.
- 使用3ω/2ω方法测量30nV以上的电信号.
- 记录的加热器和传感器温度信号高达30kHz用于数据分析.
主要成果:
- 在高真空下 (2 × 10-6 mbar) 连续66小时运行UHT-VPS从300K到1150K.
- 确定/微电阻的线性和二次温度系数.
- 测量了散装蓝宝石的热导率和热扩散率,其热导率值无法通过光学方法获得.
结论:
- 在前所未有的温度水平下,UHT-VPS为材料的同时电气和热性质检索提供了有效的解决方案.
- 该系统能够在极端条件下进行长期稳定的测量,证实其在材料研究中的实用性.
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