在不含Mo的钢原子探测器断层图像中令人惊的C行为
William Mottay1, Jeremy Landes1,2, Alain Portavoce1
1CNRS, IM2NP, Aix Marseille Université, Campus de Saint-Jérôme, Avenue Escadrille Normandie Niemen, Case 142, Marseille 13397, France.
概括
在钢中脱位时的碳分离只在共分离时观察到. 这项研究表明,原子探头断层扫描 (APT) 可能不准确地测量铁中的碳,因为在分析过程中样本会出现脱位.
科学领域:
- 材料科学
- 金属工程
- 分析化学
背景情况:
- 原子探头断层扫描 (APT) 是分析结晶缺陷中的溶液原子分离的一个关键技术.
- 了解工业钢中的溶液分离对于材料性能和性能至关重要.
研究的目的:
- 在使用APT的工业钢材等级中调查碳 (C) 分离的意外观察.
- 确定其他元素,特别是 (Mo),对C分离的影响.
- 在特定条件下评估APT测量碳的准确性.
主要方法:
- 原子探头断层扫描 (APT) 用于分析钢样中的溶液原子分布.
- 使用传输电子显微镜 (TEM) 对APT尖端进行相关分析.
- 对无钢的APT体积中的碳成分进行了统计分析.
主要成果:
- 只有在有共分离的情况下,才能观察到脱位的碳分离.
- 在没有的钢中,35%的APT体积显示了固体溶液中的碳含量是预期的5倍.
- 相对的TEM-APT分析证实没有碳分离在没有的脱位.
结论:
- 原子探针断层测量铁中的碳分离可能是不准确的.
- 在APT中使用的高电场可能会导致样本脱离,从而导致错误的碳测量.
- 在APT分析期间观察到的碳分离中,起着关键作用.
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