对于页岩油井的温度敏感丢失循环材料的准备,性能研究和现场应用实践
Wenzhe Zhang1,2, Jinsheng Sun1,3, Feng Shen2
1School of Petroleum Engineering, China University of Petroleum (East China), Qingdao 266580, China.
Polymers
|September 13, 2025
概括
开发了新型温度敏感的丢失循环材料 (TS-LCM) 颗粒,以有效密封石油和天然气井的断裂. 这些形状记忆聚合物颗粒膨胀并适应密封未知的断裂宽度,显著提高堵塞成功率并降低钻井成本.
科学领域:
- 材料科学 材料科学 材料科学
- 石油工程是石油工程中的一个.
- 聚合物化学 聚合物化学
背景情况:
- 钻井流体在形成空洞中的损失增加了运营成本和非生产时间.
- 传统的流失循环材料通常是无效的,当损失区域的大小是未知的.
- 开发先进的材料对于减轻钻井流体损失至关重要.
研究的目的:
- 为了合成和描述新型的温度敏感的流失循环材料 (TS-LCM) 颗粒.
- 评估TS-LCM的密封性能和自适应密封机制.
- 评估TS-LCM在页岩油井的现场应用中的有效性.
主要方法:
- 使用双A (DGEBA) 和4,4'-二氨基二甲的二氧化甘乙烯和4,4'-二氨基二甲合成TS-LCM粒子.
- 通过里埃变换红外光谱学分析分子结构.
- 使用差分扫描热量计 (DSC) 评估热性质 (玻璃过渡温度).
- 在高温和高压条件下使用专用测试装置评估形状记忆性质,膨胀,机械强度和密封性能.
主要成果:
- TS-LCM颗粒的玻璃过渡温度 (Tg) 为70.24°C,形状恢复在Tg以上.
- 激活的TS-LCM颗粒从状扩展到立方体形状,有效地弥合和密封高达4毫米宽的断裂,而无需事先了解宽度.
- 实地测试显示,堵塞成功率显著增加 (从32%增加到82.5%),钻井周期时间缩短 (平均14.3%).
结论:
- 开发的TS-LCM颗粒为破裂形成中的流体损失控制提供了高效和适应性的解决方案.
- TS-LCM与盐水式钻井流体具有很好的兼容性,并显著提高了井口的完整性.
- 该材料显示出在石油和天然气行业广泛应用的巨大潜力,特别是在具有挑战性的钻探环境中.
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