一种灵敏的方法,通过反应细胞的感应合等离子体质谱仪来确定大气中的二氧化硫
Qi-Xuan Sun1, Bo Li1, Xiao-Ping Kong1
1Henan Institute of Metrology, Zhengzhou, Henan, People's Republic of China.
一种新方法使用感应合等离子体质谱法 (ICP-MS) 来检测气体样本中的二氧化硫 (SO2). 这种敏感的技术实现了较低的检测极限,有助于环境监测.
科学领域:
- 分析化学 分析化学
- 环境科学 环境科学
背景情况:
- 二氧化硫 (SO2) 是一个主要的空气污染物.
- 准确的SO2测定对于环境监测至关重要.
研究的目的:
- 开发一种使用ICP-MS测定SO2的敏感方法.
- 从气体样本中优化SO2的预度技术.
主要方法:
- 使用反应细胞诱导合等离子体质谱法 (ICP-MS).
- 从气体样本中预先缩的SO2变成溶液.
- 研究的最佳O2流量,采样流量,溶液体积,吸收瓶和溶液成分.
主要成果:
- 达到了0.11ppb的检测极限 (LOD).
- 在0.7 ml min-1的最佳O2流速确定为m/z 48.
- 在大气SO2分析中表现出有利的选择性.
结论:
- 开发的ICP-MS方法为SO2的确定提供了高灵敏度和选择性.
- 这种技术对监测气态环境污染物的监测有希望.
更多相关视频
08:37Measurement of H2S in Crude Oil and Crude Oil Headspace Using Multidimensional Gas Chromatography, Deans Switching and Sulfur-selective Detection
Published on: December 10, 2015
07:57Quantitative Detection of Trace Explosive Vapors by Programmed Temperature Desorption Gas Chromatography-Electron Capture Detector
Published on: July 25, 2014
相关概念视频
Gas Chromatography: Types of Detectors-II
Inductively Coupled Plasma–Mass Spectrometry (ICP–MS): Overview
Inductively Coupled Plasma Atomic Emission Spectroscopy: Principle
The ions and electrons produced interact with the fluctuating magnetic field created by a water-cooled...
Atomic Emission Spectroscopy: Lab
Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation
There are three main types of inductively coupled plasma atomic emission spectroscopy (ICP-AES) instruments: sequential, simultaneous multichannel, and Fourier transform instruments, with the latter being less commonly used....
Atomic Emission Spectroscopy: Instrumentation
