生物活性多的高级回收:对梨种子副产品的干燥和绿色提取的综合优化
Jorge G Figueroa1,2, Isabel Borrás-Linares1, Jesús Lozano-Sánchez3
1Department of Analytical Chemistry, University of Granada, Avda. Fuente Nueva s/n, 18071 Granada, Spain.
Food chemistry: X
|December 1, 2025
概括
在200°C使用乙醇:水 (50:50) 提取梨副产品的优化加速溶剂提取 (ASE).有效回收的化合物. 种子 (85°C) 和种子外层 (75°C) 的最佳干燥温度为最大的产量而有所不同.
科学领域:
- 食品化学 食品化学
- 自然产品提取 提取自然产品
- 分析化学 分析化学
背景情况:
- 梨的种子和种子外是有价值的化合物的丰富来源.
- 需要有效的提取方法来利用这些农业副产品.
- 了解干燥和提取对型的影响至关重要.
研究的目的:
- 为了优化梨种子和种子外衣中的化合物的加速溶剂提取 (ASE) 条件.
- 为了确定梨种子和种子外样本的最佳干燥温度.
- 使用HPLC-TOF-MS识别和量化化合物.
主要方法:
- 响应表面方法与中央复合材料设计被用于优化.
- 使用乙醇:水 (50:50v/v) 在200°C进行加速溶剂提取 (ASE).
- 高性能液体色谱与飞行时间质谱 (HPLC-TOF-MS) 用于化合物分析.
主要成果:
- 两个矩阵的最佳ASE条件被确定为200°C与乙醇:水 (50:50v/v).
- 梨种子的最佳干燥温度为85°C.
- 种子外套的烯酸提取显示出最佳温度因化合物组而异,75°C对大多数最有利.
结论:
- 优化的ASE和干燥条件使梨副产品中的化合物能够有效地回收.
- 鉴定和量化了大量的化合物 (42种在种子中,52种在种子外中).
- 这项研究有助于通过有效的植物化学提取对梨废物流的价值化.
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