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磁性MON@COF复合材料用于有效检测水中的NSAID

Wei Zhao¹, Shijie Huang², Wenjie Liu³

¹Key Laboratory of Advanced Mass Spectrometry and Molecular Analysis of Zhejiang Province, School of Material Science and Chemical Engineering, Ningbo University, Ningbo 315211 Zhejiang, China.

Journal of chromatography. A

|December 3, 2025

概括

研究人员开发了新的磁性复合材料 (MMON-Br@COF) 用于检测水中的非类固醇抗炎药物 (NSAID). 这种磁性微孔有机网络和共价有机框架复合物有效吸附和检测NSAID,为环境监测提供了有前途的解决方案.

科学领域:

环境化学环境化学
材料科学材料科学材料科学
分析化学分析化学

背景情况:

剩余的非类固醇抗炎药物 (NSAIDs) 在水体中造成越来越多的环境问题.
吸附和检测NSAID的有效方法对于环境保护至关重要.

研究的目的:

为了合成新的磁性微孔有机网络和共价有机框架 (MON@COF) 复合物用于NSAID检测.
评估这些复合物的吸附性能和机制,用于常见的NSAIDs.
建立一种敏感且有效的方法,用于在水生环境中检测NSAID.

主要方法:

磁性MON@COF复合材料 (MMON-Br@COF和MMON-I@COF) 的合成.
使用高性能液体染色学 (HPLC) 评估NSAID吸附.
对吸附动力学,异热,热力学和机制的分析.
开发一种磁性固相提取与HPLC (MSPE-HPLC) 方法相结合的方法.

主要成果:

MMON-Br@COF表现出高吸附能力 (461.60 mg g-1 对于二二).
吸附遵循伪二次动力学和弗洛伊德利希等温模型,由π-π堆叠,结合和静电相互作用驱动.
开发的MSPE-HPLC方法显示了高回收率 (>87.12%),低检测极限 (0.045-0.110 μg l-1),以及出色的线性.

结论:

磁性MON@COF复合材料对于NSAID的吸附和检测是有效的.
MON和COF组件之间的协同作用提高了NSAID捕获效率.
这项研究提出了一种可行的方法,用于在水环境中去除和监测NSAID.

关键词:

吸附机制是一种吸附机制.共价有机框架是共价有机框架.微孔的有机网络是微孔的有机网络.无抗炎药 (NSAIDs) 是一种无抗炎药.痕迹检测检测器可以检测.

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