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化ZnO纳米粒子的高级XRD峰值扩展分析用于结晶体尺寸评估

Ali Khorsand Zak^1,2, Abd Manaf Hashim³

¹Nanobiotechnology Lab, Central Lab, Esfarayen University of Technology, Esfarayen, 96619-98195, North Khorasan, Iran. alikhorsandzak@gmail.com.

Scientific reports

|December 10, 2025

概括

经过修改的大小-菌株图 (MSSP) 方法准确地确定了氧化纳米粒子 (ZnO-NPs) 中的结晶体大小和晶格菌株. 较高的兴奋剂降低了晶体的尺寸,并增加了这些纳米材料的晶格应变.

科学领域:

材料科学材料科学材料科学
纳米技术纳米技术
固态物理固态物理

背景情况:

氧化纳米粒子 (ZnO-NPs) 在各种应用中至关重要.
控制结晶体大小和格子应变对于优化 ZnO-NP 特性至关重要.
兴奋剂是一种有前途的策略,可以调整ZnO-NP的特性.

研究的目的:

评估不同X射线衍射 (XRD) 分析方法的可靠性,以确定结晶体大小和晶格应变.
为了研究不同度的氧化物纳米粒子 (ZnO-NPs) 的微观结构演变.
确定纳米级材料表征的最准确方法.

主要方法:

使用凝辅助sol-gel方法合成具有不同Ga度 (0-15%) 的ZnO-NP.
通过X射线衍射 (XRD) 进行结构性表征.
使用雪勒方程,威廉森-霍尔 (W-H),大小-菌株图 (SSP) 和修改的大小-菌株图 (MSSP) 技术进行晶石大小和格子应变分析.

主要成果:

在ZnO-NPs中增加的兴奋剂导致了结晶体尺寸的减少.
较高的Ga度导致ZnO-NPs内的格子应变增加.
与其他方法相比,MSSP方法在区分尺寸和应变效应方面表现出更高的准确性.

结论:

修改的大小-菌株图 (MSSP) 技术是最可靠的方法来表征纳米材料中的晶体体大小和晶格菌株.
加的结合显著影响ZnO纳米颗粒的结构性质,导致更小的晶体和更高的晶格应变.
这项研究为准确的纳米级材料分析提供了强大的方法.

关键词:

加添加剂 ZnO 的.峰值的扩大峰值的扩大 XRD XRD 在线观看氧化的氧化是什么 ZnO ZnO ZnO ZnO ZnO ZnO ZnO ZnO ZnO ZnO ZnO ZnO

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