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为检测氨基的质量控制而制备冷牛奶参考材料
Shulin Wei1, Wei Zhang1, Decheng Suo1
1Institute of Quality Standards and Testing Technology for Agro-Products, Chinese Academy of Agricultural Sciences, Beijing 100081, China.
Veterinary sciences
|February 26, 2026
概括
开发了一种含有阿莫西西林的新牛奶参考材料,以达到最大残留量限制 (MRL). 这种经过认证的材料可确保在乳制品中检测出阿莫西西林的准确测试和质量控制.
科学领域:
- 分析化学 分析化学
- 食品安全 食品安全
- 兽医医学 兽医医学 兽医医学
背景情况:
- 氨基是牛中广泛使用的抗生素.
- 准确检测牛奶中的阿莫西西林残留物对于公共卫生和监管合规性至关重要.
- 现有的方法需要可靠的参考材料来验证和质量控制.
研究的目的:
- 为了生产和表征牛奶参考材料的阿莫西西林.
- 确定阿莫西西林在最大残留量限制 (MRL) 的认证值.
- 支持对阿莫西西林残留分析的方法验证和内部质量控制.
主要方法:
- 从用阿莫西西林处理的牛奶中生产参考材料.
- 正宗牛奶样品的冷干燥,稀释和同质化.
- 验证同位素稀释液体染色学/并联质谱法 (ID-LC/MS/MS) 方法.
主要成果:
- 牛奶参考材料被发现是均和稳定的.
- 认证值为 (4.10 ± 0.13) μg/kg,符合4.0 μg/kg的MRL.
- 相对标准偏差在2.93%至5.29%之间.
结论:
- 目前已有针对阿莫西西林的经过验证的牛奶参考材料.
- 这种参考材料有助于准确测试阿莫西西林残留物,并符合国际MRL.
- 它是食品安全实验室方法验证和质量保证的宝贵工具.
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